tert-butyl phenyl(5-phenylpent-4-yn-1-yl)carbamate

Base Information

Chemical Name:tert-butyl phenyl(5-phenylpent-4-yn-1-yl)carbamate
CAS No.:1432629-43-0
Molecular Formula:C₂₂H₂₅NO₂
Molecular Weight:335.446
Hs Code.:

Synonyms:tert-butyl phenyl(5-phenylpent-4-yn-1-yl)carbamate

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Chemical Property of tert-butyl phenyl(5-phenylpent-4-yn-1-yl)carbamate

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Technology Process of tert-butyl phenyl(5-phenylpent-4-yn-1-yl)carbamate

There total 3 articles about tert-butyl phenyl(5-phenylpent-4-yn-1-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 591-50-4
iodobenzene

: 1432629-39-4
tert-butyl pent-4-yn-1-yl(phenyl)carbamate

: 1432629-43-0
tert-butyl phenyl(5-phenylpent-4-yn-1-yl)carbamate

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In tetrahydrofuran; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2013.01.003

Reference yield:

: N-(pent-4-yn-1-yl)aniline

: 1432629-43-0
tert-butyl phenyl(5-phenylpent-4-yn-1-yl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: tert-butyl alcohol / 16 h / 0 - 20 °C / Inert atmosphere

2: bis-triphenylphosphine-palladium(II) chloride; triethylamine; copper(l) iodide / tetrahydrofuran / 20 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In tetrahydrofuran; tert-butyl alcohol;
DOI:10.1016/j.tet.2013.01.003

Reference yield:

: 110936-96-4
4-pentinoic acid anilide

: 1432629-43-0
tert-butyl phenyl(5-phenylpent-4-yn-1-yl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 30 h / 0 - 20 °C / Inert atmosphere

2: tert-butyl alcohol / 16 h / 0 - 20 °C / Inert atmosphere

3: bis-triphenylphosphine-palladium(II) chloride; triethylamine; copper(l) iodide / tetrahydrofuran / 20 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; lithium aluminium tetrahydride; triethylamine; In tetrahydrofuran; tert-butyl alcohol;
DOI:10.1016/j.tet.2013.01.003