hexyl trityl ether

Base Information

• Chemical Name: hexyl trityl ether
• CAS No.: 85058-11-3
• Molecular Formula: C₂₅H₂₈O
• Molecular Weight: 344.497
• Mol file: 85058-11-3.mol

Synonyms:hexyl trityl ether

Chemical Property of hexyl trityl ether

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of hexyl trityl ether

There total 2 articles about hexyl trityl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

trityl chloride (76-83-5) + hexan-1-ol (111-27-3) → hexyl trityl ether (85058-11-3)

Guidance literature:

With dmap; triethylamine; In dichloromethane; at 20 ℃;

DOI:10.1016/j.tet.2016.10.020

Reference yield: 42.0%

triphenylmethyl alcohol (76-84-6) + triethyl-hexyloxy-silane (18107-40-9) → hexyl trityl ether (85058-11-3)

Guidance literature:

With copper(ll) bromide; In acetonitrile; at 20 ℃; for 22h; Inert atmosphere;

DOI:10.1016/j.tetlet.2011.08.148

Reference yield: 72.0%

hexyl trityl ether (85058-11-3) → hexan-1-ol (111-27-3)

Guidance literature:

With lithium chloride; In methanol; for 12h; Reflux;

DOI:10.1016/j.tetlet.2016.06.110

upstream raw materials:

triphenylmethyl alcohol

triethyl-hexyloxy-silane

trityl chloride

hexan-1-ol

Downstream raw materials:

hexan-1-ol

trityl chloride

(decyloxymethanetriyl)tribenzene

Refernces

• 1、 Specklin, Simon,Gallier, Florian,Mezaache, Rofia,Harkat, Hassina,Dembelé, Yénimégué Albert,Weibel, Jean-Marc,Blanc, Aurélien,Pale, Patrick. "Copper(II) bromide as efficient catalyst for silyl- to bisarylmethyl ethers interconversion (transprotection)". experimental part. p. 5820 - 5823. Retrieved 2011/12/03.