(S)-2-(3-Trifluoromethyl-benzylcarbamoyl)-pyrrolidine-1-carboxylic acid 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-1,1-dimethyl-undecyl ester

Base Information

Chemical Name:(S)-2-(3-Trifluoromethyl-benzylcarbamoyl)-pyrrolidine-1-carboxylic acid 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-1,1-dimethyl-undecyl ester
CAS No.:350717-13-4
Molecular Formula:C₂₇H₂₄F₂₀N₂O₃
Molecular Weight:804.467
Hs Code.:

(S)-2-(3-Trifluoromethyl-benzylcarbamoyl)-pyrrolidine-1-carboxylic acid 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-1,1-dimethyl-undecyl ester

Synonyms:(S)-2-(3-Trifluoromethyl-benzylcarbamoyl)-pyrrolidine-1-carboxylic acid 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-1,1-dimethyl-undecyl ester

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Chemical Property of (S)-2-(3-Trifluoromethyl-benzylcarbamoyl)-pyrrolidine-1-carboxylic acid 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-1,1-dimethyl-undecyl ester

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Technology Process of (S)-2-(3-Trifluoromethyl-benzylcarbamoyl)-pyrrolidine-1-carboxylic acid 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-1,1-dimethyl-undecyl ester

There total 5 articles about (S)-2-(3-Trifluoromethyl-benzylcarbamoyl)-pyrrolidine-1-carboxylic acid 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-1,1-dimethyl-undecyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 2740-83-2
3-(TRIFLUOROMETHYL)BENZYLAMINE

: 350716-71-1
(2S)-pyrrolidine-1,2-dicarboxylic acid 1-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-1,1-dimethylundecyl) ester

: 350717-13-4
(S)-2-(3-Trifluoromethyl-benzylcarbamoyl)-pyrrolidine-1-carboxylic acid 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-1,1-dimethyl-undecyl ester

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In chloroform; N,N-dimethyl-formamide; at 20 ℃; for 16h;
DOI:10.1021/jo010111w

Reference yield:

: 2-[2-(1H,1H,2H,2H-perfluorodecyl)isopropoxycarbonyloxyimino]-2-phenylacetonitrile

: 350717-13-4
(S)-2-(3-Trifluoromethyl-benzylcarbamoyl)-pyrrolidine-1-carboxylic acid 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-1,1-dimethyl-undecyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 47 percent / Et₃N / tetrahydrofuran; H₂O / 20 °C

2: 87 percent / EDCI; HOBt; Et₃N / CHCl₃; dimethylformamide / 16 h / 20 °C

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; chloroform; water; N,N-dimethyl-formamide;
DOI:10.1021/jo010111w

Reference yield:

: 147-85-3,25191-13-3,37159-97-0,4305-67-3,4607-28-7
L-proline

: 350717-13-4
(S)-2-(3-Trifluoromethyl-benzylcarbamoyl)-pyrrolidine-1-carboxylic acid 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-1,1-dimethyl-undecyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 47 percent / Et₃N / tetrahydrofuran; H₂O / 20 °C

2: 87 percent / EDCI; HOBt; Et₃N / CHCl₃; dimethylformamide / 16 h / 20 °C

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; chloroform; water; N,N-dimethyl-formamide;
DOI:10.1021/jo010111w