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4a-(3,4-dimethoxyphenyl)-6,6-(ethylenedioxy)-2-methyl-3-oxo-2,3,4,4a,5,6,7,8-octahydroisoquinoline

Base Information Edit
  • Chemical Name:4a-(3,4-dimethoxyphenyl)-6,6-(ethylenedioxy)-2-methyl-3-oxo-2,3,4,4a,5,6,7,8-octahydroisoquinoline
  • CAS No.:88176-88-9
  • Molecular Formula:C20H25NO5
  • Molecular Weight:359.422
  • Hs Code.:
  • Mol file:88176-88-9.mol
4a-(3,4-dimethoxyphenyl)-6,6-(ethylenedioxy)-2-methyl-3-oxo-2,3,4,4a,5,6,7,8-octahydroisoquinoline

Synonyms:4a-(3,4-dimethoxyphenyl)-6,6-(ethylenedioxy)-2-methyl-3-oxo-2,3,4,4a,5,6,7,8-octahydroisoquinoline

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The product has achieved commercial mass production*data from LookChem market partment
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Chemical Property of 4a-(3,4-dimethoxyphenyl)-6,6-(ethylenedioxy)-2-methyl-3-oxo-2,3,4,4a,5,6,7,8-octahydroisoquinoline Edit
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Technology Process of 4a-(3,4-dimethoxyphenyl)-6,6-(ethylenedioxy)-2-methyl-3-oxo-2,3,4,4a,5,6,7,8-octahydroisoquinoline

There total 12 articles about 4a-(3,4-dimethoxyphenyl)-6,6-(ethylenedioxy)-2-methyl-3-oxo-2,3,4,4a,5,6,7,8-octahydroisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 9 steps
1: 1) n-BuLi, 2) glacial acetic acid, 10percent aq. HCl / 1a) ether/hexane, -60 deg C, 1 h, 1b) RT, overnight
2: pyridinium p-toluenesulfonate / benzene / 120 h / Heating
3: 1) B2H6, 2) 3N NaOH, 30 percent H2O2 / 1) THF, RT, overnight, 2a) 45 deg C, 5 h, 2b) RT
4: sodium acetate, pyridinium chlorochromate / CH2Cl2
5: 1) NaH / 1) DME, 3 h, RT, 2a) RT, overnight, 2b) 3 h, reflux
6: NaIO4/KMnO4/K2CO3 / dioxane; H2O / 48 h / Ambient temperature
7: 1N KOH / ethanol / 2 h / Heating
8: 100 percent / sodium acetate / ethanol / 40 h / Heating
9: 40 percent / p-toluenesulfonyl chloride / pyridine; H2O / 1 h / Ambient temperature
With hydrogenchloride; potassium hydroxide; sodium hydroxide; potassium permanganate; sodium periodate; n-butyllithium; dihydrogen peroxide; sodium acetate; pyridinium p-toluenesulfonate; sodium hydride; potassium carbonate; acetic acid; p-toluenesulfonyl chloride; pyridinium chlorochromate; diborane; In 1,4-dioxane; pyridine; ethanol; dichloromethane; water; benzene;
DOI:10.1021/jo00194a026
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