1-<5-Benzyloxycarbonyl-3-(2-methoxycarbonylethyl)-4-methoxycarbonylmethylpyrrol-2-yl>-3-<4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethylpyrrol-2-yl>propane-2,2-dicarbonitrile

Base Information

Chemical Name:1-<5-Benzyloxycarbonyl-3-(2-methoxycarbonylethyl)-4-methoxycarbonylmethylpyrrol-2-yl>-3-<4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethylpyrrol-2-yl>propane-2,2-dicarbonitrile
CAS No.:101210-31-5
Molecular Formula:C₃₅H₃₈N₄O₁₀
Molecular Weight:674.708
Hs Code.:

1-<5-Benzyloxycarbonyl-3-(2-methoxycarbonylethyl)-4-methoxycarbonylmethylpyrrol-2-yl>-3-<4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethylpyrrol-2-yl>propane-2,2-dicarbonitrile

Synonyms:1-<5-Benzyloxycarbonyl-3-(2-methoxycarbonylethyl)-4-methoxycarbonylmethylpyrrol-2-yl>-3-<4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethylpyrrol-2-yl>propane-2,2-dicarbonitrile

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Chemical Property of 1-<5-Benzyloxycarbonyl-3-(2-methoxycarbonylethyl)-4-methoxycarbonylmethylpyrrol-2-yl>-3-<4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethylpyrrol-2-yl>propane-2,2-dicarbonitrile

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Technology Process of 1-<5-Benzyloxycarbonyl-3-(2-methoxycarbonylethyl)-4-methoxycarbonylmethylpyrrol-2-yl>-3-<4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethylpyrrol-2-yl>propane-2,2-dicarbonitrile

There total 8 articles about 1-<5-Benzyloxycarbonyl-3-(2-methoxycarbonylethyl)-4-methoxycarbonylmethylpyrrol-2-yl>-3-<4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethylpyrrol-2-yl>propane-2,2-dicarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 101210-50-8
1-<5-Benzyloxycarbonyl-3-(2-methoxycarbonylethyl)-4-methyloxycarbonylmethylpyrrol-2-yl>-3-<5-iodo-4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethylpyrrol-2-yl>-2,2-dicyanopropane-2,2-dicarbonitrile

: 101210-31-5
1-<5-Benzyloxycarbonyl-3-(2-methoxycarbonylethyl)-4-methoxycarbonylmethylpyrrol-2-yl>-3-<4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethylpyrrol-2-yl>propane-2,2-dicarbonitrile

Guidance literature:: With hydrogen; sodium acetate; palladium on activated charcoal; for 0.666667h; Ambient temperature;

Reference yield:

: 101210-29-1
5-Chloromethyl-3-(2-methoxycarbonyl-ethyl)-4-methoxycarbonylmethyl-1H-pyrrole-2-carboxylic acid tert-butyl ester

: 101210-31-5
1-<5-Benzyloxycarbonyl-3-(2-methoxycarbonylethyl)-4-methoxycarbonylmethylpyrrol-2-yl>-3-<4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethylpyrrol-2-yl>propane-2,2-dicarbonitrile

Guidance literature:: Multi-step reaction with 4 steps

1: Huenig's base

2: CF₃COOH

3: iodination

4: H₂, NaOAc / Pd-C

With hydrogen; sodium acetate; trifluoroacetic acid; palladium on activated charcoal;
DOI:10.1039/c39850001294

Reference yield:

: 101210-49-5
1--3-<5-carboxy-4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethylpyrrol-2-yl>propane-2,2-dicarbonitrile

: 101210-31-5
1-<5-Benzyloxycarbonyl-3-(2-methoxycarbonylethyl)-4-methoxycarbonylmethylpyrrol-2-yl>-3-<4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethylpyrrol-2-yl>propane-2,2-dicarbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: iodination

2: H₂, NaOAc / Pd-C

With hydrogen; sodium acetate; palladium on activated charcoal;
DOI:10.1039/c39850001294