N⁷-benzyl-N¹,N¹³-diformyl-N⁴,N¹⁰-ditosyl-4,7,10-triaza-1,13-tridecanediamine

Base Information

• Chemical Name: N⁷-benzyl-N¹,N¹³-diformyl-N⁴,N¹⁰-ditosyl-4,7,10-triaza-1,13-tridecanediamine
• CAS No.: 164912-99-6
• Molecular Formula: C₃₃H₄₅N₅O₆S₂
• Molecular Weight: 671.882

Synonyms:N⁷-benzyl-N¹,N¹³-diformyl-N⁴,N¹⁰-ditosyl-4,7,10-triaza-1,13-tridecanediamine

Chemical Property of N⁷-benzyl-N¹,N¹³-diformyl-N⁴,N¹⁰-ditosyl-4,7,10-triaza-1,13-tridecanediamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N⁷-benzyl-N¹,N¹³-diformyl-N⁴,N¹⁰-ditosyl-4,7,10-triaza-1,13-tridecanediamine

There total 3 articles about N⁷-benzyl-N¹,N¹³-diformyl-N⁴,N¹⁰-ditosyl-4,7,10-triaza-1,13-tridecanediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

N,N-dimethyl-formamide (68-12-2,33513-42-7) + N7-benzyl-1,13-diphthalimido-N4,N10-ditosyl-4,7,10-triazatridecane (164912-95-2) → N7-benzyl-N1,N13-diformyl-N4,N10-ditosyl-4,7,10-triaza-1,13-tridecanediamine (164912-99-6)

Guidance literature:

With hydrazine hydrate; at 75 ℃; for 48h;

DOI:10.1246/bcsj.73.693

Reference yield:

N-(2-bromo-ethyl)-4-methyl-benzenesulfonamide (4556-90-5) → N7-benzyl-N1,N13-diformyl-N4,N10-ditosyl-4,7,10-triaza-1,13-tridecanediamine (164912-99-6)

Guidance literature:

Multi-step reaction with 3 steps

1: 99 percent / sodium hydrogen carbonate / acetonitrile / 96 h / 70 °C

2: 99 percent / potassium carbonate / dimethylformamide / 96 h / 20 °C

3: 95 percent / hydrazine hydrate / 48 h / 75 °C

With sodium hydrogencarbonate; potassium carbonate; hydrazine hydrate; In N,N-dimethyl-formamide; acetonitrile; 1: Alkylation / 2: Alkylation / 3: Formylation;

DOI:10.1246/bcsj.73.693

Reference yield:

N3-benzyl-N1,N5-ditosyl-3-aza-1,5-pentanediamine (112193-79-0) → N7-benzyl-N1,N13-diformyl-N4,N10-ditosyl-4,7,10-triaza-1,13-tridecanediamine (164912-99-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 99 percent / potassium carbonate / dimethylformamide / 96 h / 20 °C

2: 95 percent / hydrazine hydrate / 48 h / 75 °C

With potassium carbonate; hydrazine hydrate; In N,N-dimethyl-formamide; 1: Alkylation / 2: Formylation;

DOI:10.1246/bcsj.73.693

upstream raw materials:

N,N-dimethyl-formamide

N⁷-benzyl-1,13-diphthalimido-N⁴,N¹⁰-ditosyl-4,7,10-triazatridecane

N-(2-bromo-ethyl)-4-methyl-benzenesulfonamide

N³-benzyl-N¹,N⁵-ditosyl-3-aza-1,5-pentanediamine

Downstream raw materials:

N¹¹-benzyl-1,21-diphthalimido-N⁴,N⁸,N¹⁴,N¹⁸-tetratosyl-4,8,11,14,18-pentaazaheneicosane

N¹¹-benzyl-N¹,N²¹-diformyl-N⁴,N⁸,N¹⁴,N¹⁸-tetratosyl-4,8,11,14,18-pentaaza-1,21-heneicosanediamine

N⁷-benzyl-N¹,N⁴,N¹⁰,N¹³-tetratosyl-4,7,10-triaza-1,13-tridecanediamine

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 164912-99-6 N⁷-benzyl-N¹,N¹³-diformyl-N⁴,N¹⁰-ditosyl-4,7,10-triaza-1,13-tridecanediamine

Send

Send

Metric Ton KG G Pound L ML

Send

Send