dimethyl (E,Z)-2,2'-(2-hydroxy-1,3-phenylene)bis-(2-(hydroxyimino)-acetate)

Base Information

Chemical Name:dimethyl (E,Z)-2,2'-(2-hydroxy-1,3-phenylene)bis-(2-(hydroxyimino)-acetate)
CAS No.:1366768-20-8
Molecular Formula:C₁₂H₁₂N₂O₇
Molecular Weight:296.236
Hs Code.:

Synonyms:dimethyl (E,Z)-2,2'-(2-hydroxy-1,3-phenylene)bis-(2-(hydroxyimino)-acetate)

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Chemical Property of dimethyl (E,Z)-2,2'-(2-hydroxy-1,3-phenylene)bis-(2-(hydroxyimino)-acetate)

Chemical Property:

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Technology Process of dimethyl (E,Z)-2,2'-(2-hydroxy-1,3-phenylene)bis-(2-(hydroxyimino)-acetate)

There total 2 articles about dimethyl (E,Z)-2,2'-(2-hydroxy-1,3-phenylene)bis-(2-(hydroxyimino)-acetate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1366768-06-0
dimethyl 2,2'-(2-hydroxy-1,3-phenylene)bis(2-oxoacetate)

: 1366768-20-8
dimethyl (E,Z)-2,2'-(2-hydroxy-1,3-phenylene)bis-(2-(hydroxyimino)-acetate)

: 1366768-19-5
dimethyl (Z,Z)-2,2'-(2-hydroxy-1,3-phenylene)bis-(2-(hydroxyimino)-acetate)

Guidance literature:: With pyridine; hydroxylamine hydrochloride; In methanol; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.bmc.2012.01.045

Reference yield:

: 1366768-05-9
dimethyl 2,2'-(2-methoxy-1,3-phenylene)bis(2-oxoacetate)

: 1366768-20-8
dimethyl (E,Z)-2,2'-(2-hydroxy-1,3-phenylene)bis-(2-(hydroxyimino)-acetate)

: 1366768-19-5
dimethyl (Z,Z)-2,2'-(2-hydroxy-1,3-phenylene)bis-(2-(hydroxyimino)-acetate)

Guidance literature:: Multi-step reaction with 2 steps

1: sodium thioethylate / N,N-dimethyl-formamide / 80 °C / Inert atmosphere

2: pyridine; hydroxylamine hydrochloride / methanol / 20 °C / Inert atmosphere

With pyridine; hydroxylamine hydrochloride; sodium thioethylate; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2012.01.045