N-(2-((tert-butyldiphenylsilyl)ethynyl)phenyl)-N-methylnitrous amide

Base Information

Chemical Name:N-(2-((tert-butyldiphenylsilyl)ethynyl)phenyl)-N-methylnitrous amide
CAS No.:1581719-70-1
Molecular Formula:C₂₅H₂₆N₂OSi
Molecular Weight:398.58
Hs Code.:

Synonyms:N-(2-((tert-butyldiphenylsilyl)ethynyl)phenyl)-N-methylnitrous amide

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Chemical Property of N-(2-((tert-butyldiphenylsilyl)ethynyl)phenyl)-N-methylnitrous amide

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Technology Process of N-(2-((tert-butyldiphenylsilyl)ethynyl)phenyl)-N-methylnitrous amide

There total 1 articles about N-(2-((tert-butyldiphenylsilyl)ethynyl)phenyl)-N-methylnitrous amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 614-00-6
N-methyl-N-nitrosoaniline

: 1377860-94-0
1-[(tert-butyldiphenylsilyl)ethynyl]-1λ3,2-benziodoxol-3(1H)-one

: 1581719-70-1
N-(2-((tert-butyldiphenylsilyl)ethynyl)phenyl)-N-methylnitrous amide

Guidance literature:: With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; zinc trifluoromethanesulfonate; In 1,2-dichloro-ethane; at 80 ℃; for 16h; under 760.051 Torr; Inert atmosphere;
DOI:10.1021/ja501910e

Reference yield: 82.0%

: 1581719-70-1
N-(2-((tert-butyldiphenylsilyl)ethynyl)phenyl)-N-methylnitrous amide

: 1581720-24-2
2-((tert-butyldiphenylsilyl)ethynyl)-N-methylaniline

Guidance literature:: With sodium tetrahydroborate; nickel(II) chloride hexahydrate; In tetrahydrofuran; for 8h; under 760.051 Torr; Reflux;
DOI:10.1021/ja501910e

Reference yield:

: 1581719-70-1
N-(2-((tert-butyldiphenylsilyl)ethynyl)phenyl)-N-methylnitrous amide

: 923270-57-9
2-methylaminophenylacetylene

Guidance literature:: Multi-step reaction with 2 steps

1: nickel(II) chloride hexahydrate; sodium tetrahydroborate / tetrahydrofuran / 8 h / 760.05 Torr / Reflux

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.25 h / 20 °C / 760.05 Torr

With sodium tetrahydroborate; nickel(II) chloride hexahydrate; tetrabutyl ammonium fluoride; In tetrahydrofuran;
DOI:10.1021/ja501910e