C₅₈H₉₄N₂O₁₂Si

Base Information

• Chemical Name: C₅₈H₉₄N₂O₁₂Si
• CAS No.: 146096-58-4
• Molecular Formula: C₅₈H₉₄N₂O₁₂Si
• Molecular Weight: 1039.48
• Mol file: 146096-58-4.mol

Synonyms:C₅₈H₉₄N₂O₁₂Si

Chemical Property of C₅₈H₉₄N₂O₁₂Si

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of C₅₈H₉₄N₂O₁₂Si

There total 3 articles about C₅₈H₉₄N₂O₁₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C52H87NO12Si → C58H94N2O12Si (146096-58-4)

Guidance literature:

Multi-step reaction with 3 steps

1: 82 percent / OsO₄, NMMO / tetrahydrofuran; H₂O

2: 78 percent / aq. NaIO₄ / tetrahydrofuran

3: 1.) AcOH, 2.) potassium triphenylborohydride / 1.) THF, 2.) THF, -78 deg C

With sodium periodate; osmium(VIII) oxide; potassium bis(trimethylsilyl)amide; acetic acid; 4-methylmorpholine N-oxide; In tetrahydrofuran; water;

DOI:10.1016/S0960-894X(98)00397-7

Reference yield:

C52H89NO14Si (214411-64-0) → C58H94N2O12Si (146096-58-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 78 percent / aq. NaIO₄ / tetrahydrofuran

2: 1.) AcOH, 2.) potassium triphenylborohydride / 1.) THF, 2.) THF, -78 deg C

With sodium periodate; potassium bis(trimethylsilyl)amide; acetic acid; In tetrahydrofuran;

DOI:10.1016/S0960-894X(98)00397-7

Reference yield:

benzylamine (100-46-9) + C51H85NO13Si (146096-57-3) → C58H94N2O12Si (146096-58-4)

Guidance literature:

With potassium bis(trimethylsilyl)amide; acetic acid; Yield given. Multistep reaction; 1.) THF, 2.) THF, -78 deg C;

DOI:10.1016/S0960-894X(98)00397-7

upstream raw materials:

benzylamine

C₅₁H₈₅NO₁₃Si

C₅₂H₈₉NO₁₄Si