20-(tert-butyldiphenylsilyloxy)-14,15-oxido-eicosa-5(Z),8(Z),11(Z),14(Z)-tetraenoic acid

Base Information

Chemical Name:20-(tert-butyldiphenylsilyloxy)-14,15-oxido-eicosa-5(Z),8(Z),11(Z),14(Z)-tetraenoic acid
CAS No.:240427-70-7
Molecular Formula:C₃₆H₅₀O₃Si
Molecular Weight:558.877
Hs Code.:

Synonyms:20-(tert-butyldiphenylsilyloxy)-14,15-oxido-eicosa-5(Z),8(Z),11(Z),14(Z)-tetraenoic acid

Suppliers and Price of 20-(tert-butyldiphenylsilyloxy)-14,15-oxido-eicosa-5(Z),8(Z),11(Z),14(Z)-tetraenoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 20-(tert-butyldiphenylsilyloxy)-14,15-oxido-eicosa-5(Z),8(Z),11(Z),14(Z)-tetraenoic acid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 20-(tert-butyldiphenylsilyloxy)-14,15-oxido-eicosa-5(Z),8(Z),11(Z),14(Z)-tetraenoic acid

There total 1 articles about 20-(tert-butyldiphenylsilyloxy)-14,15-oxido-eicosa-5(Z),8(Z),11(Z),14(Z)-tetraenoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 240427-64-9
methyl 20-(tert-butyldiphenylsilyloxy)-eicosa-5(Z),8(Z),11(Z),14(Z)-tetraenoate

: 240427-70-7
20-(tert-butyldiphenylsilyloxy)-14,15-oxido-eicosa-5(Z),8(Z),11(Z),14(Z)-tetraenoic acid

Guidance literature:: With lithium hydroxide; In tetrahydrofuran; at 20 ℃; for 12h;

Reference yield: 65.0%

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 240427-70-7
20-(tert-butyldiphenylsilyloxy)-14,15-oxido-eicosa-5(Z),8(Z),11(Z),14(Z)-tetraenoic acid

: 622842-19-7
methyl 20-(tert-butyldiphenylsilyloxy)-14,15-oxido-eicosa-5(Z),8(Z),11(Z)-trienoate

Guidance literature:: 20-(tert-butyldiphenylsilyloxy)-14,15-oxido-eicosa-5(Z),8(Z),11(Z),14(Z)-tetraenoic acid; With 1,1'-carbonyldiimidazole; In dichloromethane; at 20 ℃; for 0.666667h;

With dihydrogen peroxide; lithium salt of imidazole; In diethyl ether; dichloromethane; at 0 ℃; for 0.0833333h;

diazomethane; In methanol; diethyl ether; at 0 ℃;

Reference yield:

: 240427-70-7
20-(tert-butyldiphenylsilyloxy)-14,15-oxido-eicosa-5(Z),8(Z),11(Z),14(Z)-tetraenoic acid

: 240427-72-9
methyl 20-(tert-butyldiphenylsilyloxy)eicosa-5(Z),8(Z),11(Z)-trien-14-ynoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1,1'-carbonyldiimidazole / CH₂Cl₂ / 0.67 h / 20 °C

1.2: H₂O₂; lithium imidazole / CH₂Cl₂; diethyl ether / 0.08 h / 0 °C

1.3: 65 percent / diethyl ether; methanol / 0 °C

With 1,1'-carbonyldiimidazole; In dichloromethane;