2-(acetylamino)-N1-butyl-5-<3-<(6-amino-9H-9-purinyl)methyl>phenyl>-4-pentynamide

Base Information

Chemical Name:2-(acetylamino)-N1-butyl-5-<3-<(6-amino-9H-9-purinyl)methyl>phenyl>-4-pentynamide
CAS No.:220582-71-8
Molecular Formula:C₂₃H₂₇N₇O₂
Molecular Weight:433.513
Hs Code.:

Synonyms:2-(acetylamino)-N1-butyl-5-<3-<(6-amino-9H-9-purinyl)methyl>phenyl>-4-pentynamide

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Chemical Property of 2-(acetylamino)-N1-butyl-5-<3-<(6-amino-9H-9-purinyl)methyl>phenyl>-4-pentynamide

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Technology Process of 2-(acetylamino)-N1-butyl-5-<3-<(6-amino-9H-9-purinyl)methyl>phenyl>-4-pentynamide

There total 3 articles about 2-(acetylamino)-N1-butyl-5-<3-<(6-amino-9H-9-purinyl)methyl>phenyl>-4-pentynamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 201041-83-0
2-Acetylamino-pent-4-ynoic acid butylamide

: 220582-68-3
9-(3-iodo-benzyl)-9H-purin-6-ylamine

: 220582-71-8
2-(acetylamino)-N1-butyl-5-<3-<(6-amino-9H-9-purinyl)methyl>phenyl>-4-pentynamide

Guidance literature:: With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triphenylphosphine; In various solvent(s); for 0.75h; Heating;
DOI:10.1016/S0040-4020(98)01053-9

Reference yield:

: 66224-66-6,66224-67-7,66224-68-8,66224-69-9,134434-48-3,134434-49-4,134454-76-5,134461-75-9
adenine

: 220582-71-8
2-(acetylamino)-N1-butyl-5-<3-<(6-amino-9H-9-purinyl)methyl>phenyl>-4-pentynamide

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / NaOH, Aliquat 336

2: 93 percent / Pd(PPh₃)4, CuI, PPh₃ / various solvent(s) / 0.75 h / Heating

With sodium hydroxide; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; Aliquat 336; triphenylphosphine; In various solvent(s);
DOI:10.1016/S0040-4020(98)01053-9

Reference yield:

: 49617-83-6
m-Iodobenzyl bromide

: 220582-71-8
2-(acetylamino)-N1-butyl-5-<3-<(6-amino-9H-9-purinyl)methyl>phenyl>-4-pentynamide

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / NaOH, Aliquat 336

2: 93 percent / Pd(PPh₃)4, CuI, PPh₃ / various solvent(s) / 0.75 h / Heating

With sodium hydroxide; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; Aliquat 336; triphenylphosphine; In various solvent(s);
DOI:10.1016/S0040-4020(98)01053-9