1,13-dibenzyloxy-3,11-di(triethylsilyloxy)-5-tert-butyldimethylsilyloxy-9-hydroxy-tridecan-7-one

Base Information Edit

Chemical Name:1,13-dibenzyloxy-3,11-di(triethylsilyloxy)-5-tert-butyldimethylsilyloxy-9-hydroxy-tridecan-7-one
CAS No.:185409-83-0
Molecular Formula:C₄₅H₈₀O₇Si₃
Molecular Weight:817.383
Hs Code.:
Mol file:185409-83-0.mol

Synonyms:1,13-dibenzyloxy-3,11-di(triethylsilyloxy)-5-tert-butyldimethylsilyloxy-9-hydroxy-tridecan-7-one

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Chemical Property of 1,13-dibenzyloxy-3,11-di(triethylsilyloxy)-5-tert-butyldimethylsilyloxy-9-hydroxy-tridecan-7-one Edit

Chemical Property:

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Technology Process of 1,13-dibenzyloxy-3,11-di(triethylsilyloxy)-5-tert-butyldimethylsilyloxy-9-hydroxy-tridecan-7-one

There total 2 articles about 1,13-dibenzyloxy-3,11-di(triethylsilyloxy)-5-tert-butyldimethylsilyloxy-9-hydroxy-tridecan-7-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 185409-68-1
(S)-5-benzyloxy-3-(triethylsiloxy)pentanal

: 185409-77-2
C₄₇H₈₃BO₄Si₂

: (3S,5S,9R,11S)-1,13-Bis-benzyloxy-5-(tert-butyl-dimethyl-silanyloxy)-9-hydroxy-3,11-bis-triethylsilanyloxy-tridecan-7-one

: 185409-83-0
1,13-dibenzyloxy-3,11-di(triethylsilyloxy)-5-tert-butyldimethylsilyloxy-9-hydroxy-tridecan-7-one

Guidance literature:: With dihydrogen peroxide; Yield given. Multistep reaction; 1.) -78 deg C, 5 h, 2.) MeOH, pH₇ buffer;
DOI:10.1016/0040-4039(96)01961-2

Reference yield:

: 85116-37-6
(-)-diisopinocamphenylborane chloride

: 185409-68-1
(S)-5-benzyloxy-3-(triethylsiloxy)pentanal

: 185409-75-0
(4S,6S)-8-benzyloxy-4-(tert-butyldimethylsiloxy)-6-(triethylsiloxy)-2-octanone

: 185409-83-0
1,13-dibenzyloxy-3,11-di(triethylsilyloxy)-5-tert-butyldimethylsilyloxy-9-hydroxy-tridecan-7-one

Guidance literature:: (-)-diisopinocamphenylborane chloride; (4S,6S)-8-benzyloxy-4-(tert-butyldimethylsiloxy)-6-(triethylsiloxy)-2-octanone;

(S)-5-benzyloxy-3-(triethylsiloxy)pentanal;