(3R,4S,5S)-3-amino-5-(3-bromo-4-hydroxy-benzyl)-1,1-dioxo-hexahydro-1λ6-thiopyran-4-ol hydrochloride

Base Information

Chemical Name:(3R,4S,5S)-3-amino-5-(3-bromo-4-hydroxy-benzyl)-1,1-dioxo-hexahydro-1λ6-thiopyran-4-ol hydrochloride
CAS No.:947320-53-8
Molecular Formula:C₁₂H₁₆BrNO₄S*ClH
Molecular Weight:386.694
Hs Code.:

Synonyms:(3R,4S,5S)-3-amino-5-(3-bromo-4-hydroxy-benzyl)-1,1-dioxo-hexahydro-1λ6-thiopyran-4-ol hydrochloride

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Chemical Property of (3R,4S,5S)-3-amino-5-(3-bromo-4-hydroxy-benzyl)-1,1-dioxo-hexahydro-1λ6-thiopyran-4-ol hydrochloride

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Technology Process of (3R,4S,5S)-3-amino-5-(3-bromo-4-hydroxy-benzyl)-1,1-dioxo-hexahydro-1λ6-thiopyran-4-ol hydrochloride

There total 1 articles about (3R,4S,5S)-3-amino-5-(3-bromo-4-hydroxy-benzyl)-1,1-dioxo-hexahydro-1λ6-thiopyran-4-ol hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 947320-05-0
(3R,4S,5S)-3-amino-5-(3-bromo-4-methoxy-benzyl)-1,1-dioxo-hexahydro-1λ6-thiopyran-4-ol hydrochloride

: 947320-53-8
(3R,4S,5S)-3-amino-5-(3-bromo-4-hydroxy-benzyl)-1,1-dioxo-hexahydro-1λ6-thiopyran-4-ol hydrochloride

Guidance literature:: (3R,4S,5S)-3-amino-5-(3-bromo-4-methoxy-benzyl)-1,1-dioxo-hexahydro-1λ6-thiopyran-4-ol hydrochloride; With boron tribromide; In dichloromethane; at 25 ℃; for 1.5h;

With water; potassium carbonate; In dichloromethane;

With hydrogenchloride; di-tert-butyl dicarbonate; triethylamine; isopropyl alcohol; more than 3 stages;

Reference yield:

: 947320-53-8
(3R,4S,5S)-3-amino-5-(3-bromo-4-hydroxy-benzyl)-1,1-dioxo-hexahydro-1λ6-thiopyran-4-ol hydrochloride

: 22924-15-8
3-ethoxybenzaldehyde

: (3S,4S,5R)-3-(3-bromo-4-hydroxy-benzyl)-5-(3-ethoxy-benzylamino)-1,1-dioxo-hexahydro-1λ6-thiopyran-4-ol trifluoroacetate

Guidance literature:: (3R,4S,5S)-3-amino-5-(3-bromo-4-hydroxy-benzyl)-1,1-dioxo-hexahydro-1λ6-thiopyran-4-ol hydrochloride; 3-ethoxybenzaldehyde; With sodium acetate; In methanol; dichloromethane; at 50 ℃; for 0.5h;

With sodium cyanoborohydride; In methanol; dichloromethane; at 25 ℃; for 2h;

With water; In methanol; dichloromethane;