C₁₂H₁₄O₂

Base Information

Chemical Name:C₁₂H₁₄O₂
CAS No.:1250362-66-3
Molecular Formula:C₁₂H₁₄O₂
Molecular Weight:190.242
Hs Code.:

C<sub>12</sub>H<sub>14</sub>O<sub>2</sub>

Synonyms:C₁₂H₁₄O₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₂H₁₄O₂

Chemical Property:

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Technology Process of C₁₂H₁₄O₂

There total 1 articles about C₁₂H₁₄O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 144828-84-2
N-methoxy-1′-(3-methoxyphenyl)-N-methylacetamide

: 1730-25-2
allylmagnesium bromide

: 1250362-66-3
C₁₂H₁₄O₂

Guidance literature:: In tetrahydrofuran; at -78 ℃; Inert atmosphere;
DOI:10.1021/ol300494q

Reference yield: 67.0%

: 1250362-66-3
C₁₂H₁₄O₂

: 1372559-30-2
C₁₂H₁₈O₃

Guidance literature:: C₁₂H₁₄O₂; With borane-THF; In tetrahydrofuran; at 0 - 23 ℃; for 2.16667h; Inert atmosphere;

With dihydrogen peroxide; In tetrahydrofuran; at 0 - 23 ℃; Inert atmosphere;
DOI:10.1021/ol300494q

Reference yield:

: 1250362-66-3
C₁₂H₁₄O₂

: 1372559-37-9
2-(3-methoxybenzyl)-2,3-dihydrofuran

Guidance literature:: Multi-step reaction with 5 steps

1.1: borane-THF / tetrahydrofuran / 2.17 h / 0 - 23 °C / Inert atmosphere

1.2: 0 - 23 °C / Inert atmosphere

2.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 18 h / 23 °C / Inert atmosphere; Molecular sieve

3.1: diisobutylaluminium hydride / dichloromethane / -78 °C / Inert atmosphere

4.1: triethylamine / tetrahydrofuran / 1 h / -50 °C / Inert atmosphere

5.1: tetrahydrofuran / 4 h / Inert atmosphere; Reflux

With tetrapropylammonium perruthennate; borane-THF; diisobutylaluminium hydride; 4-methylmorpholine N-oxide; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol300494q