Technology Process of C35H36N6O9S
There total 21 articles about C35H36N6O9S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C13H10BrNO4; C22H29N5O6S;
With
potassium hydrogencarbonate;
In
1,2-dimethoxyethane;
at 20 ℃;
for 16h;
Inert atmosphere;
With
pyridine; trifluoroacetic anhydride;
In
1,2-dimethoxyethane;
at 0 ℃;
for 3h;
Inert atmosphere;
With
triethylamine;
In
1,2-dimethoxyethane;
at 20 ℃;
for 3h;
Inert atmosphere;
DOI:10.1016/j.tetlet.2012.05.105
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: Lawessons reagent / 1,2-dimethoxyethane / 60 °C / Inert atmosphere
2.1: potassium hydrogencarbonate / 1,2-dimethoxyethane / 16 h / 20 °C / Inert atmosphere
2.2: 3 h / 0 °C / Inert atmosphere
2.3: 3 h / 20 °C / Inert atmosphere
With
Lawessons reagent; potassium hydrogencarbonate;
In
1,2-dimethoxyethane;
2.1: Hantzsch thiazole synthesis / 2.2: Hantzsch thiazole synthesis / 2.3: Hantzsch thiazole synthesis;
DOI:10.1016/j.tetlet.2012.05.105
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: ammonium hydroxide / methanol; water / 20 °C / Sonication
2.1: Lawessons reagent / 1,2-dimethoxyethane / 60 °C / Inert atmosphere
3.1: potassium hydrogencarbonate / 1,2-dimethoxyethane / 16 h / 20 °C / Inert atmosphere
3.2: 3 h / 0 °C / Inert atmosphere
3.3: 3 h / 20 °C / Inert atmosphere
With
Lawessons reagent; ammonium hydroxide; potassium hydrogencarbonate;
In
methanol; 1,2-dimethoxyethane; water;
3.1: Hantzsch thiazole synthesis / 3.2: Hantzsch thiazole synthesis / 3.3: Hantzsch thiazole synthesis;
DOI:10.1016/j.tetlet.2012.05.105
