bis(η5-cyclopentadienyl)(C6H5){(thiophenyl)(trimethylsilyl)methyl}zirconium

Base Information

Chemical Name:bis(η5-cyclopentadienyl)(C6H5){(thiophenyl)(trimethylsilyl)methyl}zirconium
CAS No.:102493-96-9
Molecular Formula:C₂₆H₃₀SSiZr
Molecular Weight:493.9
Hs Code.:

Synonyms:bis(η5-cyclopentadienyl)(C6H5){(thiophenyl)(trimethylsilyl)methyl}zirconium

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Chemical Property of bis(η5-cyclopentadienyl)(C6H5){(thiophenyl)(trimethylsilyl)methyl}zirconium

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Technology Process of bis(η5-cyclopentadienyl)(C6H5){(thiophenyl)(trimethylsilyl)methyl}zirconium

There total 1 articles about bis(η5-cyclopentadienyl)(C6H5){(thiophenyl)(trimethylsilyl)methyl}zirconium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 102493-94-7
bis(η5-cyclopentadienyl){(phenylthio)(trimethylsilyl)methyl}zirconium(Cl)

: 102493-96-9
bis(η5-cyclopentadienyl)(C6H5){(thiophenyl)(trimethylsilyl)methyl}zirconium

Guidance literature:: With phenylmagnesium bromide; In diethyl ether; N2-atmosphere, addn. of PhMgBr to Zr-complex, stirring (absence of light, overnight); solvent removal (vac.), extn. (pentane), solvent removal (vac.); elem. anal.;

Reference yield: 83.0%

: 102493-96-9
bis(η5-cyclopentadienyl)(C6H5){(thiophenyl)(trimethylsilyl)methyl}zirconium

: 111005-11-9
bis(η5-cyclopentadienyl)(phenylthio){(phenyl)(trimethylsilyl)methyl}zirconium

Guidance literature:: In toluene; Under protective gas, soln. of Cp2ZrC6H5(CH(SC6H5)(Si(CH3)3)) in toluene is thermolyzed (82°C, 2 d).; Volatiles are removed in vac., addn. of pentane, resulting soln. is washed with pentane, pentane removed under vac., elem. anal..;