2-amino-2-{2-[4-(5-iodohex-5-enyloxy)phenyl]ethyl}propane-1,3-diol hydrochloride

Base Information

Chemical Name:2-amino-2-{2-[4-(5-iodohex-5-enyloxy)phenyl]ethyl}propane-1,3-diol hydrochloride
CAS No.:1301696-72-9
Molecular Formula:C₁₇H₂₆INO₃*ClH
Molecular Weight:455.764
Hs Code.:

Synonyms:2-amino-2-{2-[4-(5-iodohex-5-enyloxy)phenyl]ethyl}propane-1,3-diol hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-amino-2-{2-[4-(5-iodohex-5-enyloxy)phenyl]ethyl}propane-1,3-diol hydrochloride

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Technology Process of 2-amino-2-{2-[4-(5-iodohex-5-enyloxy)phenyl]ethyl}propane-1,3-diol hydrochloride

There total 4 articles about 2-amino-2-{2-[4-(5-iodohex-5-enyloxy)phenyl]ethyl}propane-1,3-diol hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 1301696-65-0
(4-{2-[4-(5-iodohex-5-enyloxy)phenyl]ethyl}-2-methyl-4,5-dihydrooxazol-4-yl)methanol

: 1301696-72-9
2-amino-2-{2-[4-(5-iodohex-5-enyloxy)phenyl]ethyl}propane-1,3-diol hydrochloride

Guidance literature:: With hydrogenchloride; water; In 1,4-dioxane; at 50 - 70 ℃; for 24h;
DOI:10.1002/cmdc.201000477

Reference yield:

: 791097-48-8
(R/S)-4-[2-(4-hydroxymethyl-2-methyl-4,5-dihydro-oxazol-4-yl)-ethyl]-phenol

: 1301696-72-9
2-amino-2-{2-[4-(5-iodohex-5-enyloxy)phenyl]ethyl}propane-1,3-diol hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 114 h / 20 - 50 °C

2: hydrogenchloride; water / 1,4-dioxane / 24 h / 50 - 70 °C

With hydrogenchloride; di-isopropyl azodicarboxylate; water; triphenylphosphine; In tetrahydrofuran; 1,4-dioxane; 1: Mitsunobu reaction;
DOI:10.1002/cmdc.201000477

Reference yield:

: 86953-63-1
5-Iodo-5-hexen-1-ol

: 1301696-72-9
2-amino-2-{2-[4-(5-iodohex-5-enyloxy)phenyl]ethyl}propane-1,3-diol hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 114 h / 20 - 50 °C

2: hydrogenchloride; water / 1,4-dioxane / 24 h / 50 - 70 °C

With hydrogenchloride; di-isopropyl azodicarboxylate; water; triphenylphosphine; In tetrahydrofuran; 1,4-dioxane; 1: Mitsunobu reaction;
DOI:10.1002/cmdc.201000477