(3R,4R)-4-phenyl-tetrahydrothiophene-3-carboxylic (1S)-camphorsultam amide

Base Information

Chemical Name:(3R,4R)-4-phenyl-tetrahydrothiophene-3-carboxylic (1S)-camphorsultam amide
CAS No.:252192-76-0
Molecular Formula:C₂₁H₂₇NO₃S₂
Molecular Weight:405.582
Hs Code.:

Synonyms:(3R,4R)-4-phenyl-tetrahydrothiophene-3-carboxylic (1S)-camphorsultam amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3R,4R)-4-phenyl-tetrahydrothiophene-3-carboxylic (1S)-camphorsultam amide

Chemical Property:

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Technology Process of (3R,4R)-4-phenyl-tetrahydrothiophene-3-carboxylic (1S)-camphorsultam amide

There total 1 articles about (3R,4R)-4-phenyl-tetrahydrothiophene-3-carboxylic (1S)-camphorsultam amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 105850-89-3
chloromethyl (trimethylsilyl)methyl sulfide

: 109053-73-8,138381-27-8,143167-59-3
(3aS,6R,7aR)-8,8-dimethyl-1-[(2E)-3-phenylprop-2-enoyl]hexahydro-3a,6-methano-2,1-benzisothiazole 2,2-dioxide

: 252192-76-0
(3R,4R)-4-phenyl-tetrahydrothiophene-3-carboxylic (1S)-camphorsultam amide

: (3S,4S)-4-phenyl-tetrahydrothiophene-3-carboxylic (1S)-camphorsultam amide

Guidance literature:: With cesium fluoride; In acetonitrile; at 0 ℃; for 96h;
DOI:10.1021/ol9910565

Reference yield: 67.0%

: 252192-76-0
(3R,4R)-4-phenyl-tetrahydrothiophene-3-carboxylic (1S)-camphorsultam amide

: 252192-81-7
(3R,4R)-4-phenyl-tetrahydrothiophene-3-carboxylic acid

Guidance literature:: With lithium hydroxide; In tetrahydrofuran; at 70 ℃; for 6h;
DOI:10.1021/ol9910565

Reference yield:

: 252192-76-0
(3R,4R)-4-phenyl-tetrahydrothiophene-3-carboxylic (1S)-camphorsultam amide

: 180854-00-6
(2R,3R)-treo-2-methyl-3-phenylbutyric acid

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / aq. LiOH / tetrahydrofuran / 6 h / 70 °C

2: Raney nickel / ethanol; H₂O / 1 h / 70 °C

With lithium hydroxide; nickel; In tetrahydrofuran; ethanol; water;
DOI:10.1021/ol9910565