cis-exo-9,12-diphenyl-10,11(o,o'-biphenylyl)-tetracyclo<6,3,1,0^2,70^9,12>dodeca-3,5,10-triene

Base Information

• Chemical Name: cis-exo-9,12-diphenyl-10,11(o,o'-biphenylyl)-tetracyclo<6,3,1,0^2,70^9,12>dodeca-3,5,10-triene
• CAS No.: 77884-54-9
• Molecular Formula: C₃₆H₂₆
• Molecular Weight: 458.602

Synonyms:cis-exo-9,12-diphenyl-10,11(o,o'-biphenylyl)-tetracyclo<6,3,1,0^2,70^9,12>dodeca-3,5,10-triene

Chemical Property of cis-exo-9,12-diphenyl-10,11(o,o'-biphenylyl)-tetracyclo<6,3,1,0^2,70^9,12>dodeca-3,5,10-triene

Chemical Property:

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Technology Process of cis-exo-9,12-diphenyl-10,11(o,o'-biphenylyl)-tetracyclo<6,3,1,0^2,70^9,12>dodeca-3,5,10-triene

There total 1 articles about cis-exo-9,12-diphenyl-10,11(o,o'-biphenylyl)-tetracyclo<6,3,1,0^2,70^9,12>dodeca-3,5,10-triene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

diethyl-4,7-diphenyl-5,6-(o,o'-biphenylyl)-11,12-diazapentacyclo<8,2,2,02,903,706,8>tetradeca-4,13-dien-11,12-dicarboxylate (77884-53-8) → cis-exo-9,12-diphenyl-10,11(o,o'-biphenylyl)-tetracyclo<6,3,1,02,709,12>dodeca-3,5,10-triene (77884-54-9)

Guidance literature:

With potassium hydroxide; In ethanol; for 48h; Heating;

DOI:10.1016/0040-4020(80)88028-8

Reference yield: 90.0%

maleic anhydride (108-31-6) + cis-exo-9,12-diphenyl-10,11(o,o'-biphenylyl)-tetracyclo<6,3,1,02,709,12>dodeca-3,5,10-triene (77884-54-9) → C40H28O3 (77884-55-0)

Guidance literature:

In chlorobenzene; for 18h;

DOI:10.1016/0040-4020(80)88028-8

upstream raw materials:

diethyl-4,7-diphenyl-5,6-(o,o'-biphenylyl)-11,12-diazapentacyclo<8,2,2,0^2,90^3,70^6,8>tetradeca-4,13-dien-11,12-dicarboxylate

Downstream raw materials:

C₄₀H₂₈O₃

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