Technology Process of 2-phenoxy-2-phenyl-4,4-(3-oxapentamethylene)-1,3-dioxa-4-azonia-2-boratacyclohexane
There total 1 articles about 2-phenoxy-2-phenyl-4,4-(3-oxapentamethylene)-1,3-dioxa-4-azonia-2-boratacyclohexane which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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With
phenol;
In
benzene;
amine oxide and PhB(OH)2 were dissolved in benzene under heating, PhOH added, mixt. heated for 10 min; product was also formed by reaction of the same amine oxide with 5,3,3-trialkyl-2-phenyloxy-2-phenyl-1-oxa-3-azonia-2-boratacyclopentanes (95-100%); benzene was evapd. under vac., residue washed with ether, recrystd. from MeCN-petroleum ether; elem. anal.;
DOI:10.1016/0022-328X(84)80698-1