3-(3-hydroxy-4-methoxyphenyl)-5-(3-methoxy-4,5-methylenedioxyphenyl)-1,2,4-triazole

Base Information

Chemical Name:3-(3-hydroxy-4-methoxyphenyl)-5-(3-methoxy-4,5-methylenedioxyphenyl)-1,2,4-triazole
CAS No.:1221717-33-4
Molecular Formula:C₁₇H₁₅N₃O₅
Molecular Weight:341.323
Hs Code.:

Synonyms:3-(3-hydroxy-4-methoxyphenyl)-5-(3-methoxy-4,5-methylenedioxyphenyl)-1,2,4-triazole

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Chemical Property of 3-(3-hydroxy-4-methoxyphenyl)-5-(3-methoxy-4,5-methylenedioxyphenyl)-1,2,4-triazole

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Technology Process of 3-(3-hydroxy-4-methoxyphenyl)-5-(3-methoxy-4,5-methylenedioxyphenyl)-1,2,4-triazole

There total 7 articles about 3-(3-hydroxy-4-methoxyphenyl)-5-(3-methoxy-4,5-methylenedioxyphenyl)-1,2,4-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 121974-58-1
3-methoxy-4,5-methylenedioxybenzoic acid hydrazide

: 1257321-31-5
3-hydroxy-4-methoxybenzenecarboximidoyl chloride

: 1221717-33-4
3-(3-hydroxy-4-methoxyphenyl)-5-(3-methoxy-4,5-methylenedioxyphenyl)-1,2,4-triazole

Guidance literature:: With sodium methylate; In methanol; at 45 ℃; Reflux;
DOI:10.1021/np1004278

Reference yield:

: 607-91-0
myristicin

: 1221717-33-4
3-(3-hydroxy-4-methoxyphenyl)-5-(3-methoxy-4,5-methylenedioxyphenyl)-1,2,4-triazole

Guidance literature:: Multi-step reaction with 6 steps

1.1: tetrabutylammomium bromide; potassium hydroxide / 0.67 h / 100 °C

2.1: pyridine; ozone / methanol; chloroform / -15 - 0 °C

3.1: ammonium hydroxide; iodine / tetrahydrofuran; water / 16 h / 20 °C

3.2: 4 h / Reflux

4.1: thionyl chloride / 3 h / Reflux

5.1: hydrazine hydrate / methanol / 6 h / Reflux

6.1: sodium methylate / methanol / 45 °C / Reflux

With pyridine; ammonium hydroxide; thionyl chloride; tetrabutylammomium bromide; iodine; sodium methylate; ozone; hydrazine hydrate; potassium hydroxide; In tetrahydrofuran; methanol; chloroform; water;
DOI:10.1021/np1004278

Reference yield:

: 487-62-7
isomyristicin

: 1221717-33-4
3-(3-hydroxy-4-methoxyphenyl)-5-(3-methoxy-4,5-methylenedioxyphenyl)-1,2,4-triazole

Guidance literature:: Multi-step reaction with 5 steps

1.1: pyridine; ozone / methanol; chloroform / -15 - 0 °C

2.1: ammonium hydroxide; iodine / tetrahydrofuran; water / 16 h / 20 °C

2.2: 4 h / Reflux

3.1: thionyl chloride / 3 h / Reflux

4.1: hydrazine hydrate / methanol / 6 h / Reflux

5.1: sodium methylate / methanol / 45 °C / Reflux

With pyridine; ammonium hydroxide; thionyl chloride; iodine; sodium methylate; ozone; hydrazine hydrate; In tetrahydrofuran; methanol; chloroform; water;
DOI:10.1021/np1004278