ethyl 7-(2-(diphenylamino)-7-(4-formylphenyl)-9H-carbazol-9-yl)heptanoate

Base Information

Chemical Name:ethyl 7-(2-(diphenylamino)-7-(4-formylphenyl)-9H-carbazol-9-yl)heptanoate
CAS No.:1448343-31-4
Molecular Formula:C₄₀H₃₈N₂O₃
Molecular Weight:594.753
Hs Code.:

Synonyms:ethyl 7-(2-(diphenylamino)-7-(4-formylphenyl)-9H-carbazol-9-yl)heptanoate

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Chemical Property of ethyl 7-(2-(diphenylamino)-7-(4-formylphenyl)-9H-carbazol-9-yl)heptanoate

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Technology Process of ethyl 7-(2-(diphenylamino)-7-(4-formylphenyl)-9H-carbazol-9-yl)heptanoate

There total 4 articles about ethyl 7-(2-(diphenylamino)-7-(4-formylphenyl)-9H-carbazol-9-yl)heptanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1448343-30-3
ethyl 7-(2-(4-(1,3-dioxolan-2-yl)phenyl)-7-(diphenylamino)-9H-carbazol-9-yl)heptanoate

: 1448343-31-4
ethyl 7-(2-(diphenylamino)-7-(4-formylphenyl)-9H-carbazol-9-yl)heptanoate

Guidance literature:: With hydrogenchloride; water; In tetrahydrofuran; for 1h; Inert atmosphere; Reflux;
DOI:10.1039/c3nj00430a

Reference yield:

: 29823-18-5
ethyl 7-bromoheptanoate

: 1448343-31-4
ethyl 7-(2-(diphenylamino)-7-(4-formylphenyl)-9H-carbazol-9-yl)heptanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 20 °C

1.2: 5.5 h / 20 °C

2.1: hydrogenchloride; water / tetrahydrofuran / 1 h / Inert atmosphere; Reflux

With hydrogenchloride; water; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil;
DOI:10.1039/c3nj00430a

Reference yield:

: 1448343-28-9
4''-(1,3-dioxolan-2-yl)-2'-nitro-N,N-diphenyl[1,1':4',1''-terphenyl]-4-amine

: 1448343-31-4
ethyl 7-(2-(diphenylamino)-7-(4-formylphenyl)-9H-carbazol-9-yl)heptanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: triphenylphosphine / 1,2-dichloro-benzene / 26 h / 160 °C / Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 20 °C

2.2: 5.5 h / 20 °C

3.1: hydrogenchloride; water / tetrahydrofuran / 1 h / Inert atmosphere; Reflux

With hydrogenchloride; water; sodium hydride; triphenylphosphine; In tetrahydrofuran; N,N-dimethyl-formamide; 1,2-dichloro-benzene; mineral oil;
DOI:10.1039/c3nj00430a