C₂₄H₂₇NO₂

Base Information

• Chemical Name: C₂₄H₂₇NO₂
• CAS No.: 160798-13-0
• Molecular Formula: C₂₄H₂₇NO₂
• Molecular Weight: 361.484
• Mol file: 160798-13-0.mol

Synonyms:C₂₄H₂₇NO₂

Chemical Property of C₂₄H₂₇NO₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₄H₂₇NO₂

There total 5 articles about C₂₄H₂₇NO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

C27H35NO2Si → C24H27NO2 + C24H27NO2 (160798-13-0)

Guidance literature:

With formic acid; for 0.25h; Heating;

Reference yield:

C20H21NO2 (160724-73-2) → C24H27NO2 (160798-13-0)

Guidance literature:

Multi-step reaction with 5 steps

1: 93 percent / PPh₃, DEAD / tetrahydrofuran / 12 h / Ambient temperature

3: 53 percent / AIBN, Bu₃SnH / benzene / 22 h / Heating

4: 92 percent / m-CPBA / CH₂Cl₂ / 2 h / Ambient temperature

5: 71 percent / 90percent HCOOH / 0.25 h / Heating

With formic acid; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane; benzene;

Reference yield:

C27H35NOSi (160724-80-1) → C24H27NO2 (160798-13-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 92 percent / m-CPBA / CH₂Cl₂ / 2 h / Ambient temperature

2: 71 percent / 90percent HCOOH / 0.25 h / Heating

With formic acid; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;

upstream raw materials:

C₂₀H₂₁NO₂

C₂₇H₃₅NOSi

C₂₇H₃₃NO₂Si

C₃₃H₃₉NOSSi

Downstream raw materials:

7α-formyl-1,2-dehydropyrrolizidone

Refernces