S-[(2,4-dioxo-1,2,3,4-tetrahydropyrimidin-5-yl)methyl] benzenecarbothioate

Base Information

Chemical Name:S-[(2,4-dioxo-1,2,3,4-tetrahydropyrimidin-5-yl)methyl] benzenecarbothioate
CAS No.:180714-62-9
Molecular Formula:C₁₂H₁₀N₂O₃S
Molecular Weight:262.289
Hs Code.:
Mol file:180714-62-9.mol

Synonyms:thiobenzoic acid S-(2,4-dioxo-1,2,3,4-tetrahydro-pyrimidin-5-ylmethyl) ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of S-[(2,4-dioxo-1,2,3,4-tetrahydropyrimidin-5-yl)methyl] benzenecarbothioate

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Technology Process of S-[(2,4-dioxo-1,2,3,4-tetrahydropyrimidin-5-yl)methyl] benzenecarbothioate

There total 2 articles about S-[(2,4-dioxo-1,2,3,4-tetrahydropyrimidin-5-yl)methyl] benzenecarbothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 51066-54-7
sodium thiobenzoate

: 1-(2,4-dioxo-1,2,3,4-tetrahydro-pyrimidin-5-ylmethyl)-pyridinium; methanesulfonate

: 180714-62-9
thiobenzoic acid S-(2,4-dioxo-1,2,3,4-tetrahydro-pyrimidin-5-ylmethyl) ester

Guidance literature:: In water; at 80 ℃; for 0.25h;
DOI:10.1021/jo960966m

Reference yield:

: 4433-40-3
5-hydroxymethyl uracil

: 180714-62-9
thiobenzoic acid S-(2,4-dioxo-1,2,3,4-tetrahydro-pyrimidin-5-ylmethyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent

2: 90 percent / H₂O / 0.25 h / 80 °C

In water; 1: Alkylation / 2: Substitution;
DOI:10.1021/jo960966m

Reference yield:

: 180714-62-9
thiobenzoic acid S-(2,4-dioxo-1,2,3,4-tetrahydro-pyrimidin-5-ylmethyl) ester

: 180714-56-1
C₃₅H₃₄N₂O₉S₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: 93 percent / LiOH / methanol

2.1: hexamethyldisilazane; (NH₄)2SO₄ / 2.5 h / Heating

2.2: SnCl₄ / acetonitrile / 1 h

With ammonium sulfate; lithium hydroxide; 1,1,1,3,3,3-hexamethyl-disilazane; In methanol; 1.1: debenzoylation; disulfide formation / 2.1: Hilbert-Johnson glycosylation / 2.2: Hilbert-Johnson glycosylation;
DOI:10.1021/jo960966m