(R)-4-Benzyloxycarbonylamino-4-(3-ethyl-3-methyl-pentylcarbamoyl)-butyric acid benzyl ester

Base Information

Chemical Name:(R)-4-Benzyloxycarbonylamino-4-(3-ethyl-3-methyl-pentylcarbamoyl)-butyric acid benzyl ester
CAS No.:137795-67-6
Molecular Formula:C₂₈H₃₈N₂O₅
Molecular Weight:482.62
Hs Code.:

Synonyms:(R)-4-Benzyloxycarbonylamino-4-(3-ethyl-3-methyl-pentylcarbamoyl)-butyric acid benzyl ester

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Chemical Property of (R)-4-Benzyloxycarbonylamino-4-(3-ethyl-3-methyl-pentylcarbamoyl)-butyric acid benzyl ester

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Technology Process of (R)-4-Benzyloxycarbonylamino-4-(3-ethyl-3-methyl-pentylcarbamoyl)-butyric acid benzyl ester

There total 1 articles about (R)-4-Benzyloxycarbonylamino-4-(3-ethyl-3-methyl-pentylcarbamoyl)-butyric acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 59486-73-6
(2R)-5-(benzyloxy)-2-{[(benzyloxy)carbonyl]amino}-5-oxopentanoic acid

: 137795-99-4
3-Ethyl-3-methyl-pentylamine

: 137795-67-6
(R)-4-Benzyloxycarbonylamino-4-(3-ethyl-3-methyl-pentylcarbamoyl)-butyric acid benzyl ester

Guidance literature:: With chloroformic acid ethyl ester; triethylamine; Multistep reaction; 1.) THF, -10 deg C, 15 min, 2.)a) THF, -10 deg C, 1 h, b) RT, 3 h;
DOI:10.1021/jm00079a003

Reference yield:

: 137795-67-6
(R)-4-Benzyloxycarbonylamino-4-(3-ethyl-3-methyl-pentylcarbamoyl)-butyric acid benzyl ester

: 136374-75-9
(R)-4-(3-Chloro-benzoylamino)-4-(3-ethyl-3-methyl-pentylcarbamoyl)-butyric acid

Guidance literature:: Multi-step reaction with 2 steps

1: H₂, H₂O / 10percent Pd/activated charcoal / methanol / 2 h / 760 Torr / Ambient temperature

2: aq. NaOH / tetrahydrofuran / 3 h / Ambient temperature

With sodium hydroxide; water; hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol;
DOI:10.1021/jm00079a003