(4aS,8aS)-3,4,4aα,5,6,7,8,8aβ-octahydro-5,5,8aβ-trimethyl-1-methylidene-2(1H)-naphthalenone

Base Information

Chemical Name:(4aS,8aS)-3,4,4aα,5,6,7,8,8aβ-octahydro-5,5,8aβ-trimethyl-1-methylidene-2(1H)-naphthalenone
CAS No.:59633-90-8
Molecular Formula:C₁₄H₂₂O
Molecular Weight:206.328
Hs Code.:

Synonyms:(4aS,8aS)-3,4,4aα,5,6,7,8,8aβ-octahydro-5,5,8aβ-trimethyl-1-methylidene-2(1H)-naphthalenone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4aS,8aS)-3,4,4aα,5,6,7,8,8aβ-octahydro-5,5,8aβ-trimethyl-1-methylidene-2(1H)-naphthalenone

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Technology Process of (4aS,8aS)-3,4,4aα,5,6,7,8,8aβ-octahydro-5,5,8aβ-trimethyl-1-methylidene-2(1H)-naphthalenone

There total 2 articles about (4aS,8aS)-3,4,4aα,5,6,7,8,8aβ-octahydro-5,5,8aβ-trimethyl-1-methylidene-2(1H)-naphthalenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 596-85-0
manool

: 59633-90-8
(4aS,8aS)-3,4,4aα,5,6,7,8,8aβ-octahydro-5,5,8aβ-trimethyl-1-methylidene-2(1H)-naphthalenone

Guidance literature:: Multi-step reaction with 8 steps

1: 38 percent / KMnO₄, MgSO₄ / acetone / 21 h / Ambient temperature

2: 95 percent / pyridinium toluene-p-sulphonate / benzene / 5 h / Heating

3: 85 percent / NaBH₄ / methanol / 10 h

4: 94 percent / pyridine / 72 h / Ambient temperature

5: 97 percent / water, pyridinium toluene-p-sulphonate / acetone / 3 h / Heating

6: 80 percent / pentane / 0 - 10 °C / Irradiation; medium pressure mercury lamp

7: 96 percent / 1,5-diazabicyclo<5.4.0>undec-5-ene / methanol / 16 h / Ambient temperature

8: 85 percent / CrO₃ / pyridine / 3 h / Ambient temperature

With pyridine; chromium(VI) oxide; sodium tetrahydroborate; potassium permanganate; water; pyridinium p-toluenesulfonate; magnesium sulfate; 1,5-Diazabicyclo[5.4.0]undec-5-ene; In pyridine; methanol; acetone; pentane; benzene;