2-[[2-(benzyloxycarbonylamino)acetyl]amino]-5-oxo-6-(1,4,5-trimethyl-3-propyl-imidazol-1-ium-2-yl)sulfanyl-hexanoic acid bromide

Base Information

Chemical Name:2-[[2-(benzyloxycarbonylamino)acetyl]amino]-5-oxo-6-(1,4,5-trimethyl-3-propyl-imidazol-1-ium-2-yl)sulfanyl-hexanoic acid bromide
CAS No.:1449280-41-4
Molecular Formula:Br*C₂₅H₃₅N₄O₆S
Molecular Weight:599.546
Hs Code.:

Synonyms:2-[[2-(benzyloxycarbonylamino)acetyl]amino]-5-oxo-6-(1,4,5-trimethyl-3-propyl-imidazol-1-ium-2-yl)sulfanyl-hexanoic acid bromide

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Chemical Property of 2-[[2-(benzyloxycarbonylamino)acetyl]amino]-5-oxo-6-(1,4,5-trimethyl-3-propyl-imidazol-1-ium-2-yl)sulfanyl-hexanoic acid bromide

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Technology Process of 2-[[2-(benzyloxycarbonylamino)acetyl]amino]-5-oxo-6-(1,4,5-trimethyl-3-propyl-imidazol-1-ium-2-yl)sulfanyl-hexanoic acid bromide

There total 2 articles about 2-[[2-(benzyloxycarbonylamino)acetyl]amino]-5-oxo-6-(1,4,5-trimethyl-3-propyl-imidazol-1-ium-2-yl)sulfanyl-hexanoic acid bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 848301-70-2
C₁₆H₁₉BrN₂O₆

: 1449280-33-4
1,4,5-trimethyl-3-propyl-1H-imidazole-2(3H)-thione

: 1449280-41-4
2-[[2-(benzyloxycarbonylamino)acetyl]amino]-5-oxo-6-(1,4,5-trimethyl-3-propyl-imidazol-1-ium-2-yl)sulfanyl-hexanoic acid bromide

Guidance literature:: In methanol; at 20 ℃; for 48h;
DOI:10.1016/j.ejmech.2013.05.018

Reference yield:

: 32900-00-8
N-methyl-N'-propyl-thiourea

: 1449280-41-4
2-[[2-(benzyloxycarbonylamino)acetyl]amino]-5-oxo-6-(1,4,5-trimethyl-3-propyl-imidazol-1-ium-2-yl)sulfanyl-hexanoic acid bromide

Guidance literature:: Multi-step reaction with 2 steps

1: hexan-1-ol / Inert atmosphere; Reflux

2: methanol / 48 h / 20 °C

In methanol; hexan-1-ol;
DOI:10.1016/j.ejmech.2013.05.018