4-(4-amino-5-chloro-2-methoxy-benzoylamino)-piperidine-1-carboxylic acid trifluoroacetate

Base Information

• Chemical Name: 4-(4-amino-5-chloro-2-methoxy-benzoylamino)-piperidine-1-carboxylic acid trifluoroacetate
• CAS No.: 1186089-31-5
• Molecular Formula: C₂HF₃O₂*C₁₃H₁₈ClN₃O₂
• Molecular Weight: 397.782

Synonyms:4-(4-amino-5-chloro-2-methoxy-benzoylamino)-piperidine-1-carboxylic acid trifluoroacetate

Chemical Property of 4-(4-amino-5-chloro-2-methoxy-benzoylamino)-piperidine-1-carboxylic acid trifluoroacetate

Chemical Property:

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Technology Process of 4-(4-amino-5-chloro-2-methoxy-benzoylamino)-piperidine-1-carboxylic acid trifluoroacetate

There total 1 articles about 4-(4-amino-5-chloro-2-methoxy-benzoylamino)-piperidine-1-carboxylic acid trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-(4-amino-5-chloro-2-methoxy-benzoylamino)-piperidine-1-carboxylic acid tert-butyl ester (768370-78-1) + trifluoroacetic acid (76-05-1) → 4-(4-amino-5-chloro-2-methoxy-benzoylamino)-piperidine-1-carboxylic acid trifluoroacetate (1186089-31-5)

Guidance literature:

In dichloromethane; methoxybenzene; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1021/jm900881j

Reference yield:

2-bromo-1-ethanesulfonic acid (26978-65-4) + 4-(4-amino-5-chloro-2-methoxy-benzoylamino)-piperidine-1-carboxylic acid trifluoroacetate (1186089-31-5) → C15H22ClN3O5S (1186089-54-2)

Guidance literature:

With sodium hydrogencarbonate; potassium iodide; In water; N,N-dimethyl-formamide; at 90 ℃; for 16h;

DOI:10.1021/jm900881j

Reference yield:

4-Bromo-1-butanol (33036-62-3) + 4-(4-amino-5-chloro-2-methoxy-benzoylamino)-piperidine-1-carboxylic acid trifluoroacetate (1186089-31-5) → C17H26ClN3O3

Guidance literature:

With triethylamine; In acetonitrile; at 65 ℃; for 16h; Inert atmosphere;

DOI:10.1021/jm900881j

upstream raw materials:

4-(4-amino-5-chloro-2-methoxy-benzoylamino)-piperidine-1-carboxylic acid tert-butyl ester

trifluoroacetic acid

Downstream raw materials:

C₂₆H₄₃ClN₄O₂

C₂₀H₃₁ClN₄O₂

C₁₅H₂₂ClN₃O₅S

C₂₄H₄₀ClN₅O₄S

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