5-(t-Butyldiphenylsilyloxy)-2-picoline

Base Information

Chemical Name:5-(t-Butyldiphenylsilyloxy)-2-picoline
CAS No.:147936-65-0
Molecular Formula:C₂₂H₂₅NOSi
Molecular Weight:347.532
Hs Code.:
DSSTox Substance ID:DTXSID501191639

Synonyms:5-(t-Butyldiphenylsilyloxy)-2-picoline;SCHEMBL9429662;SGKVIWRYMVLRGT-UHFFFAOYSA-N;DTXSID501191639;147936-65-0;5-[[(1,1-Dimethylethyl)diphenylsilyl]oxy]-2-methylpyridine

Suppliers and Price of 5-(t-Butyldiphenylsilyloxy)-2-picoline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 5-(t-Butyldiphenylsilyloxy)-2-picoline

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:5
Exact Mass:347.170540955
Heavy Atom Count:25
Complexity:389

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=NC=C(C=C1)O[Si](C2=CC=CC=C2)(C3=CC=CC=C3)C(C)(C)C

Technology Process of 5-(t-Butyldiphenylsilyloxy)-2-picoline

There total 2 articles about 5-(t-Butyldiphenylsilyloxy)-2-picoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1121-78-4
5-Hydroxy-2-methylpyridine

: 58479-61-1
tert-butylchlorodiphenylsilane

: 147936-65-0
5-<<(1,1-Dimethylethyl)diphenylsilyl>oxy>-2-methylpyridine

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; for 12h; Ambient temperature;
DOI:10.1021/jo00101a056

Reference yield:

: 288-32-4
1H-imidazole

: 1121-78-4
5-Hydroxy-2-methylpyridine

: 58479-61-1
tert-butylchlorodiphenylsilane

: 147936-65-0
5-<<(1,1-Dimethylethyl)diphenylsilyl>oxy>-2-methylpyridine

Guidance literature:: In dichloromethane;

Reference yield: 51.0%

: 147936-65-0
5-<<(1,1-Dimethylethyl)diphenylsilyl>oxy>-2-methylpyridine

: 159150-95-5
2-(Bromomethyl)-5-<<(1,1-dimethylethyl)diphenylsilyl>oxy>pyridine

Guidance literature:: With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In tetrachloromethane; at 50 ℃; for 24h;
DOI:10.1021/jo00101a056