(8R,9S,E)-1-hydroxy-8-isopropyl-10-methyl-6-[(R)-N-methyl-S-phenylsulfonimidoyl]-9-(triethylsilyloxy)undec-6-en-5-one

Base Information

Chemical Name:(8R,9S,E)-1-hydroxy-8-isopropyl-10-methyl-6-[(R)-N-methyl-S-phenylsulfonimidoyl]-9-(triethylsilyloxy)undec-6-en-5-one
CAS No.:1608469-16-4
Molecular Formula:C₂₈H₄₉NO₄SSi
Molecular Weight:523.853
Hs Code.:

Synonyms:(8R,9S,E)-1-hydroxy-8-isopropyl-10-methyl-6-[(R)-N-methyl-S-phenylsulfonimidoyl]-9-(triethylsilyloxy)undec-6-en-5-one

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Chemical Property of (8R,9S,E)-1-hydroxy-8-isopropyl-10-methyl-6-[(R)-N-methyl-S-phenylsulfonimidoyl]-9-(triethylsilyloxy)undec-6-en-5-one

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Technology Process of (8R,9S,E)-1-hydroxy-8-isopropyl-10-methyl-6-[(R)-N-methyl-S-phenylsulfonimidoyl]-9-(triethylsilyloxy)undec-6-en-5-one

There total 1 articles about (8R,9S,E)-1-hydroxy-8-isopropyl-10-methyl-6-[(R)-N-methyl-S-phenylsulfonimidoyl]-9-(triethylsilyloxy)undec-6-en-5-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 542-28-9,26354-94-9
3,4,5,6-tetrahydro-2H-pyran-2-one

: 918637-19-1
C₂₃H₄₁NO₂SSi

: 1608469-16-4
(8R,9S,E)-1-hydroxy-8-isopropyl-10-methyl-6-[(R)-N-methyl-S-phenylsulfonimidoyl]-9-(triethylsilyloxy)undec-6-en-5-one

Guidance literature:: C₂₃H₄₁NO₂SSi; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 0 ℃; for 3h; Inert atmosphere; Schlenk technique;

3,4,5,6-tetrahydro-2H-pyran-2-one; In tetrahydrofuran; hexane; at -78 ℃; for 2h; Inert atmosphere; Schlenk technique;
DOI:10.1002/ejoc.201301461 DOI:10.1002/ejoc.201301461

Reference yield: 82.0%

: 1608469-16-4
(8R,9S,E)-1-hydroxy-8-isopropyl-10-methyl-6-[(R)-N-methyl-S-phenylsulfonimidoyl]-9-(triethylsilyloxy)undec-6-en-5-one

: 1608469-18-6
(2S,3R,6R)-2,3-diisopropyl-5-[(S)-N-methyl-S-phenylsulfonimidoyl]-1,7-dioxaspiro[5.5]undec-4-ene

Guidance literature:: With toluene-4-sulfonic acid; In 2,2,2-trifluoroethanol; at 20 ℃; for 3h; Inert atmosphere; Schlenk technique;
DOI:10.1002/ejoc.201301461