C₁₇H₂₁ClINSi

Base Information

Chemical Name:C₁₇H₂₁ClINSi
CAS No.:1260425-66-8
Molecular Formula:C₁₇H₂₁ClINSi
Molecular Weight:429.803
Hs Code.:

Synonyms:C₁₇H₂₁ClINSi

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Chemical Property of C₁₇H₂₁ClINSi

Chemical Property:

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Technology Process of C₁₇H₂₁ClINSi

There total 5 articles about C₁₇H₂₁ClINSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1232693-03-6
2-((4-chlorophenyl)diisopropylsilyl)pyridine

: 1260425-66-8
C₁₇H₂₁ClINSi

Guidance literature:: With N-iodo-succinimide; [bis(acetoxy)iodo]benzene; palladium diacetate; In 1,2-dichloro-ethane; at 70 ℃; for 1.2h; regioselective reaction; Inert atmosphere;
DOI:10.1002/anie.201004426

Reference yield:

: 109-04-6
2-bromo-pyridine

: 1260425-66-8
C₁₇H₂₁ClINSi

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / hexanes; diethyl ether / 0.67 h / -78 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: potassium phosphate; di-μ-chlorobis(norbornadiene)dirhodium(I) / 1,4-dioxane / 20 °C / Inert atmosphere

3.1: N-iodo-succinimide; [bis(acetoxy)iodo]benzene; palladium diacetate / 1,2-dichloro-ethane / 1.2 h / 70 °C / Inert atmosphere

With potassium phosphate; N-iodo-succinimide; n-butyllithium; di-μ-chlorobis(norbornadiene)dirhodium(I); [bis(acetoxy)iodo]benzene; palladium diacetate; In 1,4-dioxane; hexanes; diethyl ether; 1,2-dichloro-ethane;
DOI:10.1002/adsc.201000975

Reference yield:

: 1232692-92-0
2-(diisopropylsilyl)pyridine

: 1260425-66-8
C₁₇H₂₁ClINSi

Guidance literature:: Multi-step reaction with 2 steps

1: potassium phosphate; di-μ-chlorobis(norbornadiene)dirhodium(I) / 1,4-dioxane / 20 °C / Inert atmosphere

2: N-iodo-succinimide; [bis(acetoxy)iodo]benzene; palladium diacetate / 1,2-dichloro-ethane / 1.2 h / 70 °C / Inert atmosphere

With potassium phosphate; N-iodo-succinimide; di-μ-chlorobis(norbornadiene)dirhodium(I); [bis(acetoxy)iodo]benzene; palladium diacetate; In 1,4-dioxane; 1,2-dichloro-ethane;
DOI:10.1002/adsc.201000975