N-<2-acetyl-2-(3,4-dimethoxyphenyl)ethyl>-(3,4-methylenedioxyphenyl)acetamide

Base Information

Chemical Name:N-<2-acetyl-2-(3,4-dimethoxyphenyl)ethyl>-(3,4-methylenedioxyphenyl)acetamide
CAS No.:134993-22-9
Molecular Formula:C₂₁H₂₃NO₆
Molecular Weight:385.417
Hs Code.:

Synonyms:N-<2-acetyl-2-(3,4-dimethoxyphenyl)ethyl>-(3,4-methylenedioxyphenyl)acetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<2-acetyl-2-(3,4-dimethoxyphenyl)ethyl>-(3,4-methylenedioxyphenyl)acetamide

Chemical Property:

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Technology Process of N-<2-acetyl-2-(3,4-dimethoxyphenyl)ethyl>-(3,4-methylenedioxyphenyl)acetamide

There total 5 articles about N-<2-acetyl-2-(3,4-dimethoxyphenyl)ethyl>-(3,4-methylenedioxyphenyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 134993-18-3
N-<2-(3,4-dimethoxyphenyl)-2-(2-methyl-1,3-dithiolan-2-yl)-ethyl>-(3,4-methylenedioxyphenyl)acetamide

: 134993-22-9
N-<2-acetyl-2-(3,4-dimethoxyphenyl)ethyl>-(3,4-methylenedioxyphenyl)acetamide

Guidance literature:: With mercury(II) perchlorate; In methanol; diethyl ether; for 1h; Ambient temperature;
DOI:10.1002/ardp.19913240504

Reference yield:

: 326-59-0
benzo[1,3]dioxol-5-yl-acetic acid methyl ester

: 134993-22-9
N-<2-acetyl-2-(3,4-dimethoxyphenyl)ethyl>-(3,4-methylenedioxyphenyl)acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / 16 h / 150 °C

2: 93 percent / Hg(ClO₄)2 trihydrate / methanol; diethyl ether / 1 h / Ambient temperature

With mercury(II) perchlorate; In methanol; diethyl ether;
DOI:10.1002/ardp.19913240504

Reference yield:

: 134993-16-1
α-(3,4-dimethoxyphenyl)-α-(2-methyl-1,3-dithiolan-2-yl)acetonitrile

: 134993-22-9
N-<2-acetyl-2-(3,4-dimethoxyphenyl)ethyl>-(3,4-methylenedioxyphenyl)acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / B₂H₆-tetrahydrofuran complex / tetrahydrofuran / 0.75 h / Heating

2: 93 percent / 16 h / 150 °C

3: 93 percent / Hg(ClO₄)2 trihydrate / methanol; diethyl ether / 1 h / Ambient temperature

With mercury(II) perchlorate; B₂H₆-THF; In tetrahydrofuran; methanol; diethyl ether;
DOI:10.1002/ardp.19913240504