(E)-2-(Benzhydrylidene-amino)-but-2-enedioic acid 1-tert-butyl ester 4-methyl ester

Base Information

Chemical Name:(E)-2-(Benzhydrylidene-amino)-but-2-enedioic acid 1-tert-butyl ester 4-methyl ester
CAS No.:126181-36-0
Molecular Formula:C₂₂H₂₃NO₄
Molecular Weight:365.429
Hs Code.:

Synonyms:(E)-2-(Benzhydrylidene-amino)-but-2-enedioic acid 1-tert-butyl ester 4-methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-2-(Benzhydrylidene-amino)-but-2-enedioic acid 1-tert-butyl ester 4-methyl ester

Chemical Property:

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Technology Process of (E)-2-(Benzhydrylidene-amino)-but-2-enedioic acid 1-tert-butyl ester 4-methyl ester

There total 1 articles about (E)-2-(Benzhydrylidene-amino)-but-2-enedioic acid 1-tert-butyl ester 4-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 126181-27-9
N-Benzhydrylidene-oxalamic acid tert-butyl ester

: 21204-67-1,2605-67-6
methyl (triphenylphosphoranylidene)acetate

: 126181-36-0
(E)-2-(Benzhydrylidene-amino)-but-2-enedioic acid 1-tert-butyl ester 4-methyl ester

: 791-28-6
Triphenylphosphine oxide

Guidance literature:: In toluene; for 12h; Heating;
DOI:10.1016/S0040-4039(00)99404-8

Reference yield: 95.0%

: 126181-36-0
(E)-2-(Benzhydrylidene-amino)-but-2-enedioic acid 1-tert-butyl ester 4-methyl ester

: 126181-41-7
2-(Benzhydryl-amino)-succinic acid 1-tert-butyl ester 4-methyl ester

Guidance literature:: With sodium cyanoborohydride; In tetrahydrofuran; acetic acid; for 24h; Heating;
DOI:10.1016/S0040-4039(00)99404-8

Reference yield:

: 126181-36-0
(E)-2-(Benzhydrylidene-amino)-but-2-enedioic acid 1-tert-butyl ester 4-methyl ester

: 1835-51-4
(RS)-2-amino-3-methoxycarbonylpropionic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / sodium cyanoborohydride / acetic acid; tetrahydrofuran / 24 h / Heating

2: 85 percent / 10percent Pd/C / acetic acid / Heating

With sodium cyanoborohydride; palladium on activated charcoal; In tetrahydrofuran; acetic acid;
DOI:10.1016/S0040-4039(00)99404-8