O-methyl S-p-methylphenyl thiocarbonate

Base Information

Chemical Name:O-methyl S-p-methylphenyl thiocarbonate
CAS No.:3186-53-6
Molecular Formula:C₉H₁₀O₂S
Molecular Weight:182.243
Hs Code.:

Synonyms:O-methyl S-p-methylphenyl thiocarbonate

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Chemical Property of O-methyl S-p-methylphenyl thiocarbonate

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Technology Process of O-methyl S-p-methylphenyl thiocarbonate

There total 2 articles about O-methyl S-p-methylphenyl thiocarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 10486-08-5
sodium p-thiocresolate

: 176794-26-6
(E)-3-(3-Bromo-2,4,6-trimethyl-phenyl)-3-chloro-2-methyl-acrylic acid methyl ester

: 103-19-5
di(p-tolyl) disulfide

: 3186-53-6
O-methyl S-p-methylphenyl thiocarbonate

: (3-bromo-2,4,6-trimethylphenyl)methylacetylene

: 2-Bromo-1,3,5-trimethyl-4-((Z)-1-p-tolylsulfanyl-propenyl)-benzene

Guidance literature:: In acetonitrile; for 48h; Product distribution; Heating; other reagents, reaction times;
DOI:10.1021/jo9600565

Reference yield:

: 3186-53-6
O-methyl S-p-methylphenyl thiocarbonate

Guidance literature:: Methoxycarbonylsulfenylchlorid 1, Toluol;

Reference yield: 85.0%

: 3186-53-6
O-methyl S-p-methylphenyl thiocarbonate

: 5122-94-1
4-biphenylboronic acid

: 720-75-2
methyl 4-phenylbenzoate

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; copper(I) thiophene-2-carboxylate; trifuran-2-yl-phosphane; In 1,4-dioxane; at 60 ℃; for 16h; Sealed tube; Inert atmosphere;
DOI:10.1021/acs.joc.0c00198