7-Acetyl-6-methyl-2,4-diphenyl-2,3,4-trihydrothiazolo<3,2-a>-1,3,5-triazine oxime

Base Information

Chemical Name:7-Acetyl-6-methyl-2,4-diphenyl-2,3,4-trihydrothiazolo<3,2-a>-1,3,5-triazine oxime
CAS No.:87102-45-2
Molecular Formula:C₂₀H₂₀N₄OS
Molecular Weight:364.471
Hs Code.:

Synonyms:7-Acetyl-6-methyl-2,4-diphenyl-2,3,4-trihydrothiazolo<3,2-a>-1,3,5-triazine oxime

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Chemical Property of 7-Acetyl-6-methyl-2,4-diphenyl-2,3,4-trihydrothiazolo<3,2-a>-1,3,5-triazine oxime

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Technology Process of 7-Acetyl-6-methyl-2,4-diphenyl-2,3,4-trihydrothiazolo<3,2-a>-1,3,5-triazine oxime

There total 4 articles about 7-Acetyl-6-methyl-2,4-diphenyl-2,3,4-trihydrothiazolo<3,2-a>-1,3,5-triazine oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 87102-33-8
1-(6-Methyl-2,4-diphenyl-3,4-dihydro-2H-thiazolo[3,2-a][1,3,5]triazin-7-yl)-ethanone

: 87102-45-2
7-Acetyl-6-methyl-2,4-diphenyl-2,3,4-trihydrothiazolo<3,2-a>-1,3,5-triazine oxime

Guidance literature:: With hydroxylamine hydrochloride; In acetic acid; for 0.5h; Heating;
DOI:10.1021/je00035a032

Reference yield:

: 61582-10-3
4,6-diphenyl[1,3,5]triazinane-2-thione

: 87102-45-2
7-Acetyl-6-methyl-2,4-diphenyl-2,3,4-trihydrothiazolo<3,2-a>-1,3,5-triazine oxime

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / 1.) 85percent KOH / ethanol / 1.) 70-80 deg C, 10 min, 2.) room temp., 18 h

2: 60 percent / polyphosphoric acid / 1.) 100 deg C, 1 h, 2.) 120 deg C, 15 min

3: 58 percent / hydroxylamine hydrochloride / acetic acid / 0.5 h / Heating

With potassium hydroxide; PPA; hydroxylamine hydrochloride; In ethanol; acetic acid;
DOI:10.1021/je00035a032

Reference yield:

: 87102-24-7
(E)-3-(4,6-Diphenyl-1,4,5,6-tetrahydro-[1,3,5]triazin-2-ylsulfanyl)-4-hydroxy-pent-3-en-2-one

: 87102-45-2
7-Acetyl-6-methyl-2,4-diphenyl-2,3,4-trihydrothiazolo<3,2-a>-1,3,5-triazine oxime

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / polyphosphoric acid / 1.) 100 deg C, 1 h, 2.) 120 deg C, 15 min

2: 58 percent / hydroxylamine hydrochloride / acetic acid / 0.5 h / Heating

With PPA; hydroxylamine hydrochloride; In acetic acid;
DOI:10.1021/je00035a032