2,5-bis(4-methoxyphenyl)-1-phenyl-N-(quinolin-8-yl)cyclopentanecarboxamide

Base Information

Chemical Name:2,5-bis(4-methoxyphenyl)-1-phenyl-N-(quinolin-8-yl)cyclopentanecarboxamide
CAS No.:1534433-50-5
Molecular Formula:C₃₅H₃₂N₂O₃
Molecular Weight:528.651
Hs Code.:

Synonyms:2,5-bis(4-methoxyphenyl)-1-phenyl-N-(quinolin-8-yl)cyclopentanecarboxamide

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Chemical Property of 2,5-bis(4-methoxyphenyl)-1-phenyl-N-(quinolin-8-yl)cyclopentanecarboxamide

Chemical Property:

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Technology Process of 2,5-bis(4-methoxyphenyl)-1-phenyl-N-(quinolin-8-yl)cyclopentanecarboxamide

There total 3 articles about 2,5-bis(4-methoxyphenyl)-1-phenyl-N-(quinolin-8-yl)cyclopentanecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17380-62-0
1-phenylcyclopentanecarboxylic acid chloride

: 1534433-50-5
2,5-bis(4-methoxyphenyl)-1-phenyl-N-(quinolin-8-yl)cyclopentanecarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 0 - 20 °C

2: nickel(II) triflate; mesitylenecarboxylic acid; sodium carbonate / N,N-dimethyl-formamide / 24 h / 160 °C / Inert atmosphere

With nickel(II) triflate; mesitylenecarboxylic acid; sodium carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja411715v

Reference yield:

: 696-62-8
para-iodoanisole

: 908520-36-5
1-phenyl-N-(quinolin-8-yl)cyclopentanecarboxamide

: 1534433-49-2
2-(4-methoxyphenyl)-1-phenyl-N-(quinolin-8-yl)cyclopentanecarboxamide

: 1534433-50-5
2,5-bis(4-methoxyphenyl)-1-phenyl-N-(quinolin-8-yl)cyclopentanecarboxamide

Guidance literature:: With nickel(II) triflate; mesitylenecarboxylic acid; sodium carbonate; In N,N-dimethyl-formamide; at 160 ℃; for 24h; Inert atmosphere;
DOI:10.1021/ja411715v

Reference yield:

: 77-55-4
1-phenyl-1-cyclopentanecarboxylic acid

: 1534433-50-5
2,5-bis(4-methoxyphenyl)-1-phenyl-N-(quinolin-8-yl)cyclopentanecarboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride / N,N-dimethyl-formamide; dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

2: triethylamine / dichloromethane / 0 - 20 °C

3: nickel(II) triflate; mesitylenecarboxylic acid; sodium carbonate / N,N-dimethyl-formamide / 24 h / 160 °C / Inert atmosphere

With nickel(II) triflate; oxalyl dichloride; mesitylenecarboxylic acid; sodium carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja411715v