tert-butyl (1R)-1-[5-(7-ethyl-1-methyl-2,2-dioxido-3,4-dihydro-1H-[1,2,5]thiadiazepino[3,4,5-hi]indol-9-yl)-1,3,4-oxadiazol-2-yl]-1-methyl-2-phenylethylcarbamate

Base Information

Chemical Name:tert-butyl (1R)-1-[5-(7-ethyl-1-methyl-2,2-dioxido-3,4-dihydro-1H-[1,2,5]thiadiazepino[3,4,5-hi]indol-9-yl)-1,3,4-oxadiazol-2-yl]-1-methyl-2-phenylethylcarbamate
CAS No.:925455-54-5
Molecular Formula:C₂₉H₃₅N₅O₅S
Molecular Weight:565.693
Hs Code.:

tert-butyl (1R)-1-[5-(7-ethyl-1-methyl-2,2-dioxido-3,4-dihydro-1H-[1,2,5]thiadiazepino[3,4,5-hi]indol-9-yl)-1,3,4-oxadiazol-2-yl]-1-methyl-2-phenylethylcarbamate

Synonyms:tert-butyl (1R)-1-[5-(7-ethyl-1-methyl-2,2-dioxido-3,4-dihydro-1H-[1,2,5]thiadiazepino[3,4,5-hi]indol-9-yl)-1,3,4-oxadiazol-2-yl]-1-methyl-2-phenylethylcarbamate

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Chemical Property of tert-butyl (1R)-1-[5-(7-ethyl-1-methyl-2,2-dioxido-3,4-dihydro-1H-[1,2,5]thiadiazepino[3,4,5-hi]indol-9-yl)-1,3,4-oxadiazol-2-yl]-1-methyl-2-phenylethylcarbamate

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Technology Process of tert-butyl (1R)-1-[5-(7-ethyl-1-methyl-2,2-dioxido-3,4-dihydro-1H-[1,2,5]thiadiazepino[3,4,5-hi]indol-9-yl)-1,3,4-oxadiazol-2-yl]-1-methyl-2-phenylethylcarbamate

There total 1 articles about tert-butyl (1R)-1-[5-(7-ethyl-1-methyl-2,2-dioxido-3,4-dihydro-1H-[1,2,5]thiadiazepino[3,4,5-hi]indol-9-yl)-1,3,4-oxadiazol-2-yl]-1-methyl-2-phenylethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 925455-53-4
tert-butyl (1R)-1-benzyl-2-{2-[(7-ethyl-1-methyl-2,2-dioxido-3,4-dihydro-1H-[1,2,5]thiadiazepino[3,4,5-hi]indol-9-yl)carbonyl]hydrazino}-1-methyl-2-oxoethylcarbamate

: 925455-54-5
tert-butyl (1R)-1-[5-(7-ethyl-1-methyl-2,2-dioxido-3,4-dihydro-1H-[1,2,5]thiadiazepino[3,4,5-hi]indol-9-yl)-1,3,4-oxadiazol-2-yl]-1-methyl-2-phenylethylcarbamate

Guidance literature:: With 1H-imidazole; carbon tetrabromide; triphenylphosphine; In dichloromethane; at 0 - 20 ℃; for 2.08333h;

Reference yield:

: 925455-54-5
tert-butyl (1R)-1-[5-(7-ethyl-1-methyl-2,2-dioxido-3,4-dihydro-1H-[1,2,5]thiadiazepino[3,4,5-hi]indol-9-yl)-1,3,4-oxadiazol-2-yl]-1-methyl-2-phenylethylcarbamate

: (2R)-2-[5-(7-ethyl-1-methyl-2,2-dioxido-3,4-dihydro-1H-[1,2,5]thiadiazepino[3,4,5-hi]indol-9-yl)-1,3,4-oxadiazol-2-yl]-1-phenylpropan-2-amine

Guidance literature:: tert-butyl (1R)-1-[5-(7-ethyl-1-methyl-2,2-dioxido-3,4-dihydro-1H-[1,2,5]thiadiazepino[3,4,5-hi]indol-9-yl)-1,3,4-oxadiazol-2-yl]-1-methyl-2-phenylethylcarbamate; With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 16h;

With sodium hydrogencarbonate; In water; ethyl acetate;