tetrakis(4-thiylphenyl)methane

Base Information

• Chemical Name: tetrakis(4-thiylphenyl)methane
• CAS No.: 361344-97-0
• Molecular Formula: C₂₅H₂₀S₄
• Molecular Weight: 448.698
• Mol file: 361344-97-0.mol

Synonyms:tetrakis(4-thiylphenyl)methane

Chemical Property of tetrakis(4-thiylphenyl)methane

Chemical Property:

Purity/Quality:

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Technology Process of tetrakis(4-thiylphenyl)methane

There total 1 articles about tetrakis(4-thiylphenyl)methane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

tetrakis(4-bromophenyl)methane (105309-59-9) → tetrakis(4-thiylphenyl)methane (361344-97-0)

Guidance literature:

tetrakis(4-bromophenyl)methane; With sodium isopropanethiolate; In N,N-dimethyl acetamide; at 100 ℃; for 16h; Inert atmosphere;

With sodium; In N,N-dimethyl acetamide; for 24h;

DOI:10.1002/adfm.201302483

Reference yield: 95.0%

tetrakis(4-thiylphenyl)methane (361344-97-0) + 1,1'-biphenyl-4,4'-diyl-bis-pyrrole-2,5-dione (3278-30-6) → C65H44N4O8S4

Guidance literature:

With acetic acid; In N,N-dimethyl-formamide; at 20 ℃; for 48h; Solvent; Sealed tube;

DOI:10.1039/c5ra01463h

Reference yield: 86.0%

maleiimide (541-59-3,25721-74-8) + tetrakis(4-thiylphenyl)methane (361344-97-0) → 3,3',3'',3'''-[(methanetetrayltetrakis(benzene-4,1-diyl))tetrakis-(sulfane diyl)]tetrakis(pyrrolidine-2,5-dione)

Guidance literature:

With triethylamine; In toluene; at 20 ℃; for 16h; Inert atmosphere;

DOI:10.1039/c5ra01463h

upstream raw materials:

tetrakis(4-bromophenyl)methane

Refernces