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C26H39N3O8

Base Information
  • Chemical Name:C26H39N3O8
  • CAS No.:1422008-62-5
  • Molecular Formula:C26H39N3O8
  • Molecular Weight:521.611
  • Hs Code.:
C<sub>26</sub>H<sub>39</sub>N<sub>3</sub>O<sub>8</sub>

Synonyms:C26H39N3O8

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Chemical Property of C26H39N3O8
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Technology Process of C26H39N3O8

There total 3 articles about C26H39N3O8 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With sodium methylate; In methanol; at 20 ℃; for 3h;
DOI:10.1016/j.bmc.2012.11.041
Guidance literature:
Multi-step reaction with 8 steps
1: sodium tetrahydroborate / tetrahydrofuran / 4 h / 20 °C
2: triethylamine / tetrahydrofuran / 0.33 h / 0 °C
3: sodium hydride / tetrahydrofuran / 10 h / 0 °C / Reflux
4: hydrazine hydrate / isopropyl alcohol / 20 °C
5: benzyltri(n-butyl)ammonium chloride; sodium hydroxide / dichloromethane / 20 °C
6: palladium 10% on activated carbon; hydrogen / methanol; water / 20 °C
7: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / water; N,N-dimethyl-formamide / 20 °C
8: sodium methylate / methanol / 3 h / 20 °C
With sodium tetrahydroborate; palladium 10% on activated carbon; hydrogen; sodium methylate; benzyltri(n-butyl)ammonium chloride; sodium hydride; benzotriazol-1-ol; hydrazine hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1016/j.bmc.2012.11.041
Guidance literature:
Multi-step reaction with 5 steps
1: hydrazine hydrate / isopropyl alcohol / 20 °C
2: benzyltri(n-butyl)ammonium chloride; sodium hydroxide / dichloromethane / 20 °C
3: palladium 10% on activated carbon; hydrogen / methanol; water / 20 °C
4: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / water; N,N-dimethyl-formamide / 20 °C
5: sodium methylate / methanol / 3 h / 20 °C
With palladium 10% on activated carbon; hydrogen; sodium methylate; benzyltri(n-butyl)ammonium chloride; benzotriazol-1-ol; hydrazine hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In methanol; dichloromethane; water; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1016/j.bmc.2012.11.041
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