ethyl 6-amino-4-<<3-(N-methyl-N-phenylamino)-2-oxopropyl>amino>-5-nitro-2-pyridinecarbamate oxime

Base Information

Chemical Name:ethyl 6-amino-4-<<3-(N-methyl-N-phenylamino)-2-oxopropyl>amino>-5-nitro-2-pyridinecarbamate oxime
CAS No.:82585-57-7
Molecular Formula:C₁₈H₂₃N₇O₅
Molecular Weight:417.425
Hs Code.:

Synonyms:ethyl 6-amino-4-<<3-(N-methyl-N-phenylamino)-2-oxopropyl>amino>-5-nitro-2-pyridinecarbamate oxime

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 6-amino-4-<<3-(N-methyl-N-phenylamino)-2-oxopropyl>amino>-5-nitro-2-pyridinecarbamate oxime

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of ethyl 6-amino-4-<<3-(N-methyl-N-phenylamino)-2-oxopropyl>amino>-5-nitro-2-pyridinecarbamate oxime

There total 2 articles about ethyl 6-amino-4-<<3-(N-methyl-N-phenylamino)-2-oxopropyl>amino>-5-nitro-2-pyridinecarbamate oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 6506-86-1
ethyl (6-amino-4-chloro-5-nitropyridin-2-yl)carbamate

: 82585-27-1
1-amino-3-(N-methyl-N-phenylamino)propanone oxime

: 82585-57-7
ethyl 6-amino-4-<<3-(N-methyl-N-phenylamino)-2-oxopropyl>amino>-5-nitro-2-pyridinecarbamate oxime

Guidance literature:: With triethylamine; In ethanol; at 75 ℃; for 24h;
DOI:10.1021/jm00351a008

Reference yield:

: 82585-29-3
2-[2-[(E)-Hydroxyimino]-3-(methyl-phenyl-amino)-propyl]-isoindole-1,3-dione

: 82585-57-7
ethyl 6-amino-4-<<3-(N-methyl-N-phenylamino)-2-oxopropyl>amino>-5-nitro-2-pyridinecarbamate oxime

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine / ethanol / 22 h / 40 °C

2: 84 percent / Et₃N / ethanol / 24 h / 75 °C

With triethylamine; hydrazine; In ethanol;
DOI:10.1021/jm00351a008