α-[4-(1-piperidinylmethyl)phenyl]-α-phenyl-1-tricyclo[3.3.1.1^3,7]decanemethanol

Base Information

• Chemical Name: α-[4-(1-piperidinylmethyl)phenyl]-α-phenyl-1-tricyclo[3.3.1.1^3,7]decanemethanol
• CAS No.: 1410789-52-4
• Molecular Formula: C₂₉H₃₇NO
• Molecular Weight: 415.619

Synonyms:α-[4-(1-piperidinylmethyl)phenyl]-α-phenyl-1-tricyclo[3.3.1.1^3,7]decanemethanol

Chemical Property of α-[4-(1-piperidinylmethyl)phenyl]-α-phenyl-1-tricyclo[3.3.1.1^3,7]decanemethanol

Chemical Property:

Purity/Quality:

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Technology Process of α-[4-(1-piperidinylmethyl)phenyl]-α-phenyl-1-tricyclo[3.3.1.1^3,7]decanemethanol

There total 4 articles about α-[4-(1-piperidinylmethyl)phenyl]-α-phenyl-1-tricyclo[3.3.1.1^3,7]decanemethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-benzoyladamantane (31919-47-8) → α-[4-(1-piperidinylmethyl)phenyl]-α-phenyl-1-tricyclo[3.3.1.13,7]decanemethanol (1410789-52-4)

Guidance literature:

Multi-step reaction with 3 steps

1.1: magnesium / diethyl ether / Inert atmosphere; Reflux

1.2: 0 °C / Inert atmosphere

2.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 8 h / Reflux

3.1: tetrahydrofuran / 10 h / Reflux

With N-Bromosuccinimide; magnesium; dibenzoyl peroxide; In tetrahydrofuran; tetrachloromethane; diethyl ether;

DOI:10.1021/jm3013008

Reference yield:

para-bromotoluene (106-38-7) → α-[4-(1-piperidinylmethyl)phenyl]-α-phenyl-1-tricyclo[3.3.1.13,7]decanemethanol (1410789-52-4)

Guidance literature:

Multi-step reaction with 3 steps

1.1: magnesium / diethyl ether / Inert atmosphere; Reflux

1.2: 0 °C / Inert atmosphere

2.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 8 h / Reflux

3.1: tetrahydrofuran / 10 h / Reflux

With N-Bromosuccinimide; magnesium; dibenzoyl peroxide; In tetrahydrofuran; tetrachloromethane; diethyl ether;

DOI:10.1021/jm3013008

Reference yield:

α-(4-methylphenyl)-α-phenyl-1-tricyclo[3.3.1.13,7]decanemethanol (102933-75-5) → α-[4-(1-piperidinylmethyl)phenyl]-α-phenyl-1-tricyclo[3.3.1.13,7]decanemethanol (1410789-52-4)

Guidance literature:

Multi-step reaction with 2 steps

1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 8 h / Reflux

2: tetrahydrofuran / 10 h / Reflux

With N-Bromosuccinimide; dibenzoyl peroxide; In tetrahydrofuran; tetrachloromethane;

DOI:10.1021/jm3013008

upstream raw materials:

1-benzoyladamantane

α-(4-methylphenyl)-α-phenyl-1-tricyclo[3.3.1.1^3,7]decanemethanol

piperidine

para-bromotoluene

Downstream raw materials:

C₂₉H₃₇N

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