N-((S)-1-Hydroxymethyl-2-methyl-propyl)-N'-{(1S,2S)-2-[((S)-1-hydroxymethyl-2-methyl-propylaminooxalyl)-amino]-cyclohexyl}-oxalamide

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Chemical Name:N-((S)-1-Hydroxymethyl-2-methyl-propyl)-N'-{(1S,2S)-2-[((S)-1-hydroxymethyl-2-methyl-propylaminooxalyl)-amino]-cyclohexyl}-oxalamide
CAS No.:910116-82-4
Molecular Formula:C₂₀H₃₆N₄O₆
Molecular Weight:428.529
Hs Code.:

Synonyms:N-((S)-1-Hydroxymethyl-2-methyl-propyl)-N'-{(1S,2S)-2-[((S)-1-hydroxymethyl-2-methyl-propylaminooxalyl)-amino]-cyclohexyl}-oxalamide

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Chemical Property of N-((S)-1-Hydroxymethyl-2-methyl-propyl)-N'-{(1S,2S)-2-[((S)-1-hydroxymethyl-2-methyl-propylaminooxalyl)-amino]-cyclohexyl}-oxalamide

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Technology Process of N-((S)-1-Hydroxymethyl-2-methyl-propyl)-N'-{(1S,2S)-2-[((S)-1-hydroxymethyl-2-methyl-propylaminooxalyl)-amino]-cyclohexyl}-oxalamide

There total 2 articles about N-((S)-1-Hydroxymethyl-2-methyl-propyl)-N'-{(1S,2S)-2-[((S)-1-hydroxymethyl-2-methyl-propylaminooxalyl)-amino]-cyclohexyl}-oxalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 910116-80-2
(1S,2S)-N,N'-1,2-cyclohexanediyl-bis(oxalamic acid ethyl ester)

: 2026-48-4,473-75-6
(S)-valinol

: 910116-82-4
N-((S)-1-Hydroxymethyl-2-methyl-propyl)-N'-{(1S,2S)-2-[((S)-1-hydroxymethyl-2-methyl-propylaminooxalyl)-amino]-cyclohexyl}-oxalamide

Guidance literature:: In toluene; for 72h; Heating;
DOI:10.1021/jo060767v

Reference yield:

: 21436-03-3
(S,S)-1,2-diaminocyclohexane

: 910116-82-4
N-((S)-1-Hydroxymethyl-2-methyl-propyl)-N'-{(1S,2S)-2-[((S)-1-hydroxymethyl-2-methyl-propylaminooxalyl)-amino]-cyclohexyl}-oxalamide

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / Et₃N / CH₂Cl₂ / 12 h / 20 °C

2: 95 percent / toluene / 72 h / Heating

With triethylamine; In dichloromethane; toluene;
DOI:10.1021/jo060767v

Reference yield: 91.0%

: 910116-82-4
N-((S)-1-Hydroxymethyl-2-methyl-propyl)-N'-{(1S,2S)-2-[((S)-1-hydroxymethyl-2-methyl-propylaminooxalyl)-amino]-cyclohexyl}-oxalamide

: N,N'-[(1S,2S)-cyclohexane-1,2-diyl]bis[(4S)-4,5-dihydro-4-(1-methylethyl)oxazole-2-carboxamide]

Guidance literature:: With (bis-(2-methoxyethyl)amino)sulfur trufluoride; In tetrahydrofuran; dichloromethane; at -10 - 20 ℃; for 5h;
DOI:10.1021/jo060767v