1-(3-Isopropenyl-2-methylene-cyclopentyloxymethyl)-4-methoxy-benzene

Base Information

• Chemical Name: 1-(3-Isopropenyl-2-methylene-cyclopentyloxymethyl)-4-methoxy-benzene
• CAS No.: 185946-09-2
• Molecular Formula: C₁₇H₂₂O₂
• Molecular Weight: 258.36
• Mol file: 185946-09-2.mol

Synonyms:1-(3-Isopropenyl-2-methylene-cyclopentyloxymethyl)-4-methoxy-benzene

Chemical Property of 1-(3-Isopropenyl-2-methylene-cyclopentyloxymethyl)-4-methoxy-benzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-(3-Isopropenyl-2-methylene-cyclopentyloxymethyl)-4-methoxy-benzene

There total 3 articles about 1-(3-Isopropenyl-2-methylene-cyclopentyloxymethyl)-4-methoxy-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

3-(4-methoxybenzyloxy)-7-methyl-oct-6-en-1-yne (131130-65-9) → 1-(3-Isopropenyl-2-methylene-cyclopentyloxymethyl)-4-methoxy-benzene (185946-09-2)

Guidance literature:

With cyclopentadienylruthenium(II) trisacetonitrile hexafluorophosphate; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

DOI:10.1021/ja993401r

Reference yield:

3-(4-methoxybenzyloxy)-7-methyl-oct-6-en-1-yne (131130-65-9) → 1-(3-Isopropylidene-2-methylene-cyclopentyloxymethyl)-4-methoxy-benzene (131130-77-3) + 1-(3-Isopropenyl-2-methylene-cyclopentyloxymethyl)-4-methoxy-benzene (185946-09-2)

Guidance literature:

With triphenyl-arsane; palladium diacetate; In benzene-d6; at 60 ℃; for 0.833333h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;

Reference yield:

3-(4-methoxybenzyloxy)-7-methyl-oct-6-en-1-yne (131130-65-9) → 1-(3-Isopropylidene-2-methylene-cyclopentyloxymethyl)-4-methoxy-benzene (131130-77-3) + 1-(3-Isopropenyl-2-methylene-cyclopentyloxymethyl)-4-methoxy-benzene (185946-09-2) + C34H44O4

Guidance literature:

With palladium diacetate; triphenylphosphine; In benzene; Product distribution; Ambient temperature; other reagents, temperature;

DOI:10.1021/ja9624937

upstream raw materials:

3-(4-methoxybenzyloxy)-7-methyl-oct-6-en-1-yne