Diallyl 2-(3,5-difluoro-4-triisopropylsilanyloxybenzyl)-2-[2-(4-methoxycarbonylphenyl)ethyl]-malonate

Base Information

Chemical Name:Diallyl 2-(3,5-difluoro-4-triisopropylsilanyloxybenzyl)-2-[2-(4-methoxycarbonylphenyl)ethyl]-malonate
CAS No.:934818-74-3
Molecular Formula:C₃₅H₄₆F₂O₇Si
Molecular Weight:644.828
Hs Code.:

Synonyms:Diallyl 2-(3,5-difluoro-4-triisopropylsilanyloxybenzyl)-2-[2-(4-methoxycarbonylphenyl)ethyl]-malonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Diallyl 2-(3,5-difluoro-4-triisopropylsilanyloxybenzyl)-2-[2-(4-methoxycarbonylphenyl)ethyl]-malonate

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Technology Process of Diallyl 2-(3,5-difluoro-4-triisopropylsilanyloxybenzyl)-2-[2-(4-methoxycarbonylphenyl)ethyl]-malonate

There total 1 articles about Diallyl 2-(3,5-difluoro-4-triisopropylsilanyloxybenzyl)-2-[2-(4-methoxycarbonylphenyl)ethyl]-malonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 934738-39-3
diallyl 2-[2-(4-methoxycarbonylphenyl)ethyl]malonate

: 934818-63-0
5-Bromomethyl-1,3-difluoro-2-triisopropylsilanyloxybenzene

: 934818-74-3
Diallyl 2-(3,5-difluoro-4-triisopropylsilanyloxybenzyl)-2-[2-(4-methoxycarbonylphenyl)ethyl]-malonate

Guidance literature:: diallyl 2-[2-(4-methoxycarbonylphenyl)ethyl]malonate; With sodium hydride; In 1,4-dioxane; mineral oil; at 0 - 20 ℃;

5-Bromomethyl-1,3-difluoro-2-triisopropylsilanyloxybenzene; In 1,4-dioxane; mineral oil; at 0 - 20 ℃;

Reference yield: 49.0%

: 934818-74-3
Diallyl 2-(3,5-difluoro-4-triisopropylsilanyloxybenzyl)-2-[2-(4-methoxycarbonylphenyl)ethyl]-malonate

: 934818-75-4
Methyl 4-[3-carboxy-4-(3,5-difluoro-4-triisopropylsilanyloxyphenyl)butyl]benzoate

Guidance literature:: With formic acid; triethylamine; triphenylphosphine; palladium diacetate; In 1,4-dioxane; at 100 ℃; for 2h; Inert atmosphere;