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2,5-dimethyl-1-tributylstannylbenzene

Base Information
  • Chemical Name:2,5-dimethyl-1-tributylstannylbenzene
  • CAS No.:192063-41-5
  • Molecular Formula:C20H36Sn
  • Molecular Weight:395.216
  • Hs Code.:
2,5-dimethyl-1-tributylstannylbenzene

Synonyms:2,5-dimethyl-1-tributylstannylbenzene

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Chemical Property of 2,5-dimethyl-1-tributylstannylbenzene
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Technology Process of 2,5-dimethyl-1-tributylstannylbenzene

There total 1 articles about 2,5-dimethyl-1-tributylstannylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With manganese; chloro-trimethyl-silane; (2,2'-bipyridine)nickel(II) dibromide; tetraethylammonium iodide; triphenylphosphine; In N,N-dimethyl-formamide; at 50 - 400 ℃; for 4h; Schlenk technique; Inert atmosphere;
DOI:10.1039/c5ob01096a
Guidance literature:
With Hg(OCOCF3)2; In chloroform; stirring Pb(OAc)4 with equimolar amt. of Sn-compd. and 0.05 equiv. Hg(OCOCF3)2 (60°C, 72 h); filtration, concn. (40°C, vac.), dissoln. in petroleum ether, crystn. (4°C, overnight), filtration, washing (petroleum ether), drying (vac.); elem. anal.;
DOI:10.1016/S0022-328X(96)06477-7
upstream raw materials:

4-bromo-m-xylene

tributyltin methoxide

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