(1S,3S,4S)-1-N-benzyl-3-tert-butyldiphenylsilyloxy-4-hydroxy-1-N-oxidopyrrolidine

Base Information

Chemical Name:(1S,3S,4S)-1-N-benzyl-3-tert-butyldiphenylsilyloxy-4-hydroxy-1-N-oxidopyrrolidine
CAS No.:959911-89-8
Molecular Formula:C₂₇H₃₃NO₃Si
Molecular Weight:447.649
Hs Code.:

Synonyms:(1S,3S,4S)-1-N-benzyl-3-tert-butyldiphenylsilyloxy-4-hydroxy-1-N-oxidopyrrolidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,3S,4S)-1-N-benzyl-3-tert-butyldiphenylsilyloxy-4-hydroxy-1-N-oxidopyrrolidine

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Technology Process of (1S,3S,4S)-1-N-benzyl-3-tert-butyldiphenylsilyloxy-4-hydroxy-1-N-oxidopyrrolidine

There total 2 articles about (1S,3S,4S)-1-N-benzyl-3-tert-butyldiphenylsilyloxy-4-hydroxy-1-N-oxidopyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 959911-84-3
(3S,4S)-N-benzyl-3,4-dihydroxy-1-N-oxidopyrrolidine

: 58479-61-1
tert-butylchlorodiphenylsilane

: 959911-89-8
(1S,3S,4S)-1-N-benzyl-3-tert-butyldiphenylsilyloxy-4-hydroxy-1-N-oxidopyrrolidine

Guidance literature:: With pyridine; at 20 ℃;
DOI:10.1016/j.tetasy.2007.08.022

Reference yield:

: 90365-74-5,330152-66-4
(3S,4S)-(+)-1-benzyl-3,4-pyrrolidinediol

: 959911-89-8
(1S,3S,4S)-1-N-benzyl-3-tert-butyldiphenylsilyloxy-4-hydroxy-1-N-oxidopyrrolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / hydrogen peroxide / ethanol; H₂O / 20 °C

2: 98 percent / pyridine / 20 °C

With pyridine; dihydrogen peroxide; In ethanol; water;
DOI:10.1016/j.tetasy.2007.08.022