1,2-Dicyclohexyl-1,2,3,4-tetrahydro-4-phenyl-3-(2-phenylethenyl)-3,6-bis(trimethylsilyloxy)-1,2-diphosphinin-1,2-disulfid

Base Information

Chemical Name:1,2-Dicyclohexyl-1,2,3,4-tetrahydro-4-phenyl-3-(2-phenylethenyl)-3,6-bis(trimethylsilyloxy)-1,2-diphosphinin-1,2-disulfid
CAS No.:93545-03-0
Molecular Formula:C₃₆H₅₄O₂P₂S₂Si₂
Molecular Weight:701.074
Hs Code.:

Synonyms:1,2-Dicyclohexyl-1,2,3,4-tetrahydro-4-phenyl-3-(2-phenylethenyl)-3,6-bis(trimethylsilyloxy)-1,2-diphosphinin-1,2-disulfid

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Chemical Property of 1,2-Dicyclohexyl-1,2,3,4-tetrahydro-4-phenyl-3-(2-phenylethenyl)-3,6-bis(trimethylsilyloxy)-1,2-diphosphinin-1,2-disulfid

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Technology Process of 1,2-Dicyclohexyl-1,2,3,4-tetrahydro-4-phenyl-3-(2-phenylethenyl)-3,6-bis(trimethylsilyloxy)-1,2-diphosphinin-1,2-disulfid

There total 2 articles about 1,2-Dicyclohexyl-1,2,3,4-tetrahydro-4-phenyl-3-(2-phenylethenyl)-3,6-bis(trimethylsilyloxy)-1,2-diphosphinin-1,2-disulfid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 93545-01-8
1,2-Dicyclohexyl-1,2,3,4-tetrahydro-4-phenyl-3-(2-phenylethenyl)-3,6-bis(trimethylsilyloxy)-1,2-diphosphinin

: 93545-03-0
1,2-Dicyclohexyl-1,2,3,4-tetrahydro-4-phenyl-3-(2-phenylethenyl)-3,6-bis(trimethylsilyloxy)-1,2-diphosphinin-1,2-disulfid

Guidance literature:: With sulfur; In benzene; at 30 ℃; for 168h;

Reference yield:

: 102-92-1,17082-09-6
cinnamoyl chloride

: 93545-03-0
1,2-Dicyclohexyl-1,2,3,4-tetrahydro-4-phenyl-3-(2-phenylethenyl)-3,6-bis(trimethylsilyloxy)-1,2-diphosphinin-1,2-disulfid

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent / pentane; toluene / 2 h / Ambient temperature

2: 63 percent / S / benzene / 168 h / 30 °C

With sulfur; In toluene; pentane; benzene;