tert-butyl N-benzyl-N-methyl-(S)-leucyl-(R)-lactyl-N-methyl-(S)-leucyl-(R)-3-phenyllactate

Base Information

• Chemical Name: tert-butyl N-benzyl-N-methyl-(S)-leucyl-(R)-lactyl-N-methyl-(S)-leucyl-(R)-3-phenyllactate
• CAS No.: 169808-78-0
• Molecular Formula: C₃₇H₅₄N₂O₇
• Molecular Weight: 638.845

Synonyms:tert-butyl N-benzyl-N-methyl-(S)-leucyl-(R)-lactyl-N-methyl-(S)-leucyl-(R)-3-phenyllactate

Chemical Property of tert-butyl N-benzyl-N-methyl-(S)-leucyl-(R)-lactyl-N-methyl-(S)-leucyl-(R)-3-phenyllactate

Chemical Property:

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Technology Process of tert-butyl N-benzyl-N-methyl-(S)-leucyl-(R)-lactyl-N-methyl-(S)-leucyl-(R)-3-phenyllactate

There total 1 articles about tert-butyl N-benzyl-N-methyl-(S)-leucyl-(R)-lactyl-N-methyl-(S)-leucyl-(R)-3-phenyllactate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

tert-butyl N-methyl-(S)-leucyl-(R)-3-phenyllactate + N-benzyl-N-methyl-(S)-leucyl-(R)-lactic acid hydrochloride → tert-butyl N-benzyl-N-methyl-(S)-leucyl-(R)-lactyl-N-methyl-(S)-leucyl-(R)-3-phenyllactate (169808-78-0)

Guidance literature:

With bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; 1.) 0 deg C, 1 h; 2.) 20 deg C, 1 h;

DOI:10.1016/0040-4020(95)00461-G

Reference yield: 74.0%

tert-butyl N-benzyl-N-methyl-(S)-leucyl-(R)-lactyl-N-methyl-(S)-leucyl-(R)-3-phenyllactate (169808-78-0) → tert-butyl N-methyl-(S)-leucyl-(R)-lactyl-N-methyl-(S)-leucyl-(R)-3-phenyllactate

Guidance literature:

With hydrogen; palladium hydroxide - carbon; In ethanol; at 20 ℃;

DOI:10.1016/0040-4020(95)00461-G

Reference yield:

tert-butyl N-benzyl-N-methyl-(S)-leucyl-(R)-lactyl-N-methyl-(S)-leucyl-(R)-3-phenyllactate (169808-78-0) → N-benzyl-N-methyl-(S)-leucyl-(R)-lactyl-N-methyl-(S)-leucyl-(R)-3-phenyllactic acid hydrochloride

Guidance literature:

With hydrogenchloride; In dichloromethane; at 20 ℃; for 12h;

DOI:10.1016/0040-4020(95)00461-G

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