2-[2-(ethoxycarbonyl)phenyl]methyl-1,3-dimethyl-4-oxo-1,4-dihydroquinazolin-3-ium perchlorate

Base Information

Chemical Name:2-[2-(ethoxycarbonyl)phenyl]methyl-1,3-dimethyl-4-oxo-1,4-dihydroquinazolin-3-ium perchlorate
CAS No.:1100083-25-7
Molecular Formula:C₂₀H₂₁N₂O₃*ClO₄
Molecular Weight:436.849
Hs Code.:

Synonyms:2-[2-(ethoxycarbonyl)phenyl]methyl-1,3-dimethyl-4-oxo-1,4-dihydroquinazolin-3-ium perchlorate

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Chemical Property of 2-[2-(ethoxycarbonyl)phenyl]methyl-1,3-dimethyl-4-oxo-1,4-dihydroquinazolin-3-ium perchlorate

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Technology Process of 2-[2-(ethoxycarbonyl)phenyl]methyl-1,3-dimethyl-4-oxo-1,4-dihydroquinazolin-3-ium perchlorate

There total 2 articles about 2-[2-(ethoxycarbonyl)phenyl]methyl-1,3-dimethyl-4-oxo-1,4-dihydroquinazolin-3-ium perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 683779-77-3
ethyl 2-[(1-methyl-4-oxo-1,4-dihydro-2-quinazolinyl)methyl]benzoate

: 80-48-8
methyl p-toluene sulfonate

: 1100083-25-7
2-[2-(ethoxycarbonyl)phenyl]methyl-1,3-dimethyl-4-oxo-1,4-dihydroquinazolin-3-ium perchlorate

Guidance literature:: ethyl 2-[(1-methyl-4-oxo-1,4-dihydro-2-quinazolinyl)methyl]benzoate; methyl p-toluene sulfonate; at 140 ℃; for 1h;

With sodium perchlorate; In ethanol; Further stages.;
DOI:10.1007/s10593-007-0197-4

Reference yield:

: 683779-64-8
ethyl 2-[(3-methyl-4-oxo-3,4-dihydro-2-quinazolinyl)methyl]benzoate

: 80-48-8
methyl p-toluene sulfonate

: 1100083-25-7
2-[2-(ethoxycarbonyl)phenyl]methyl-1,3-dimethyl-4-oxo-1,4-dihydroquinazolin-3-ium perchlorate

Guidance literature:: ethyl 2-[(3-methyl-4-oxo-3,4-dihydro-2-quinazolinyl)methyl]benzoate; methyl p-toluene sulfonate; at 140 ℃; for 1h;

With sodium perchlorate; In ethanol; Further stages.;
DOI:10.1007/s10593-007-0197-4