C₁₉H₁₈INO

Base Information

Chemical Name:C₁₉H₁₈INO
CAS No.:1392323-54-4
Molecular Formula:C₁₉H₁₈INO
Molecular Weight:403.263
Hs Code.:

Synonyms:C₁₉H₁₈INO

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Chemical Property of C₁₉H₁₈INO

Chemical Property:

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Technology Process of C₁₉H₁₈INO

There total 2 articles about C₁₉H₁₈INO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 39212-27-6
N-benzoyl cyclohexenyl-2 aniline

: 1392323-54-4
C₁₉H₁₈INO

Guidance literature:: With 3BF₄^(1-)*C₃₆H₅₈IN₄⁽³⁺⁾; (Ra)-4-hydroxy-2,6-bis(2,4,6-triisopropylphenyl)-9,14-bis(triisopropylsilyl)dinaphtho[1,3,2]dioxaphosphepine 4-oxide; sodium phosphate; In hexane; para-xylene; at 20 ℃; for 16h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ja305795x

Reference yield:

: 141091-37-4
2-(cyclohex-1-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1392323-54-4
C₁₉H₁₈INO

Guidance literature:: Multi-step reaction with 2 steps

1: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; palladium diacetate / 1,4-dioxane; water / 12 h / 90 °C / Inert atmosphere

2: 3BF₄^(1-)*C₃₆H₅₈IN₄⁽³⁺⁾; (Ra)-4-hydroxy-2,6-bis(2,4,6-triisopropylphenyl)-9,14-bis(triisopropylsilyl)dinaphtho[1,3,2]dioxaphosphepine 4-oxide; sodium phosphate / hexane; para-xylene / 16 h / 20 °C / Inert atmosphere

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; 3BF₄^(1-)*C₃₆H₅₈IN₄⁽³⁺⁾; (Ra)-4-hydroxy-2,6-bis(2,4,6-triisopropylphenyl)-9,14-bis(triisopropylsilyl)dinaphtho[1,3,2]dioxaphosphepine 4-oxide; palladium diacetate; sodium phosphate; In 1,4-dioxane; hexane; para-xylene; water;
DOI:10.1021/ja305795x